US EPA Method 8082: GC Analysis of Aroclor 1016/1260 (PCBs) on SLB®-5ms
Materiały
Standardowe
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Cennik
Pesticide Surrogate Spike Mix
certified reference material, TraceCERT®, 200 μg/mL each component in acetone, ampule of 1 mLkolumna analityczna
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polecane
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prekolumna
wymagane, ale niedostarczone
wyposażenie dodatkowe
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Cennik
Wheaton wide-mouth bottle
amber soda-lime glass bottle, capacity 1000 mL, white polypropylene cap, (PTFE faced LDPE liner), case of 12 eaCONDITIONS
column
SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)
oven
100 °C (2 min), 15 °C/min to 330 °C (3 min)
inj. temp.
250 °C
detector
ECD, 330 °C
carrier gas
helium, 25 cm/sec, constant
injection
2 μL splitless (0.75 min)
liner
4 mm I.D., single taper
sample
Aroclor standard mix 1 (46846-U) diluted to 500 ppb / 50 ppb (Aroclors / surrogates) in n-hexane
Opis
Komentarz do analizy
Aroclors are commercial mixtures of PCB congeners. Due to their stability, they ave been used in many different industrial and commercial applications. Because of their toxicity and ability to bioaccumulate, production of these materials ceased in 1977. This application demonstrates the separation of two common Aroclor mixtures, Aroclor 1016 and Aroclor 1260 on the SLB-5ms.
Informacje prawne
SLB is a registered trademark of Merck KGaA, Darmstadt, Germany