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US EPA Method 8082: GC Analysis of Aroclor 1016/1260 (PCBs) on SLB^®-5ms

US EPA Method 8082: GC Analysis of Aroclor 1016/1260 (PCBs) on SLB®-5ms suitable for GC

材料

ガードカラム

製品番号

詳細

価格

25740-U

無極性フューズドシリカチューブ

L × I.D. 5.0 m × 0.10 mm

25742

無極性フューズドシリカチューブ

L × I.D. 5.0 m × 0.25 mm

25744

無極性フューズドシリカチューブ

L × I.D. 5.0 m × 0.53 mm

付属品

製品番号

詳細

価格

Z250228

Wheaton wide-mouth bottle

amber soda-lime glass bottle, capacity 1000 mL, white polypropylene cap, (PTFE faced LDPE liner), case of 12 ea

分析カラム

製品番号

詳細

価格

24103-U

SPB^®-608キャピラリーGCカラム

L × I.D. 30 m × 0.25 mm, d_f 0.25 μm

25312

SPB^®-608キャピラリーGCカラム

L × I.D. 30 m × 0.53 mm, d_f 0.50

28372-U

Equity-1701キャピラリーGCカラム

L × I.D. 30 m × 0.25 mm, d_f 0.25 μm

28378-U

Equity-1701キャピラリーGCカラム

L × I.D. 30 m × 0.25 mm, d_f 1.00 μm

28391-U

Equity-1701キャピラリーGCカラム

L × I.D. 30 m × 0.53 mm, d_f 0.50 μm

28471-U

SLB^®-5msキャピラリーGCカラム

L × I.D. 30 m × 0.25 mm, d_f 0.25 μm

28476-U

SLB^®-5msキャピラリーGCカラム

L × I.D. 30 m × 0.25 mm, d_f 1.00 μm

28466-U

SLB^®-5msキャピラリーGCカラム

L × I.D. 15 m × 0.10 mm, d_f 0.10 μm

必要ですが提供されていません

製品番号

詳細

価格

20480

"Y" GlasSealコネクター、ボロシリカガラス

pkg of 1 ea

23631

"Y" GlasSealコネクター、融合シリカ

pkg of 1 ea

23632

"Y" GlasSealコネクター、融合シリカ

pkg of 3 ea

推奨

製品番号

詳細

価格

23817

ポリイミドシール材樹脂

pkg of 5 g

標準

製品番号

詳細

価格

44805

Aroclor 1232 溶液

certified reference material, 1000 μg/mL in isooctane

44806

Aroclor 1242 溶液

certified reference material, 1000 μg/mL in isooctane

44807

Aroclor 1248 溶液

certified reference material, 1000 μg/mL in isooctane

44808

Aroclor 1254 溶液

certified reference material, 1000 μg/mL in isooctane

44809

Aroclor 1260 溶液

certified reference material, 1000 μg/mL in isooctane

44810

Aroclor 1262 溶液

certified reference material, 1000 μg/mL in isooctane

48098

Aroclor 1221 溶液

certified reference material, 1000 μg/mL in isooctane

48707

Aroclor 1254 溶液

certified reference material, 200 μg/mL in methanol

46846-U

AroclorスタンダードMix 1

certified reference material, in acetone: methanol (2:3) (varied)

48097

Aroclor 1016 溶液

certified reference material, 1000 μg/mL in isooctane

CRM48460

農薬サロゲート添加用Mix

certified reference material, TraceCERT^®, 200 μg/mL each component in acetone, ampule of 1 mL

CONDITIONS

column

SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)

oven

100 °C (2 min), 15 °C/min to 330 °C (3 min)

inj. temp.

250 °C

detector

ECD, 330 °C

carrier gas

helium, 25 cm/sec, constant

injection

2 μL splitless (0.75 min)

liner

4 mm I.D., single taper

sample

Aroclor standard mix 1 (46846-U) diluted to 500 ppb / 50 ppb (Aroclors / surrogates) in n-hexane

詳細

アナリシスノート

Aroclors are commercial mixtures of PCB congeners. Due to their stability, they ave been used in many different industrial and commercial applications. Because of their toxicity and ability to bioaccumulate, production of these materials ceased in 1977. This application demonstrates the separation of two common Aroclor mixtures, Aroclor 1016 and Aroclor 1260 on the SLB-5ms.

法的情報

SLB is a registered trademark of Merck KGaA, Darmstadt, Germany

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