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20724AST

Supelco

Astec® CYCLOBOND I 2000 DMP Chiral HPLC Column

5 μm particle size, L × I.D. 25 cm × 4.6 mm

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About This Item

Código UNSPSC:
41115700
eCl@ss:
32110501
NACRES:
SB.52

Materiais

stainless steel column

Nível de qualidade

linha de produto

Astec®

embalagem

pkg of 1 ea

fabricante/nome comercial

Astec®

Parâmetros

0-50 °C temperature
172 bar pressure (2500 psi)

técnica(s)

HPLC: suitable
LC/MS: suitable

C × D.I.

25 cm × 4.6 mm

matriz

silica particle platform
fully porous particle

Grupo ativo da matriz

cyclodextrin, beta- phase

tamanho de partícula

5 μm

tamanho de poro

100 Å

pH operacional

3.5-7

técnica de separação

chiral

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Descrição geral

The reaction of the 3,5-dimethylphenyl isocyanate with the hydroxyl groups of β-cyclodextrin results in a pi-basic phase similar in character to the naphthylethyl carbamate phases. The selectivity is greater for the CYCLOBOND I 2000 DMP when the chiral center of the analyte is part of a ring structure or is on the α carbon. This phase has been very useful for derivatized amines, like amphetamine ACQ.

  • Bonded phase: 3,5-Dimethylphenyl carbamate modified β-cyclodextrin

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Informações legais

Astec is a registered trademark of Merck KGaA, Darmstadt, Germany

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Indirect photodetection of pregnanolone on a Cyclobond column by high-performance liquid chromatography
Agnus, Benoit, et al.
Journal of Chromatography A, 633 (1), 27-33 (1994)
Rapid high-performance liquid chromatographic separation of barley malt a-amylase on cyclobond columns
Henson, Cynthia A., Stone, Julie M.
Journal of Chromatography A, 469, 361-367 (1989)
Reprint of: Enantiomeric separation of functionalized ethano-bridged Troger bases using macrocyclic cyclofructan and cyclodextrin chiral selectors in high-performance liquid chromatography and capillary electrophoresis with application of principal component analysis
Weatherly, Choyce A., et al.
Journal of Chromatography. B, Biomedical Applications, 968, 40-48 (2014)
Enantiomeric separation of functionalized ethano-bridged Troger bases using macrocyclic cyclofructan and cyclodextrin chiral selectors in high-performance liquid chromatography and capillary electrophoresis with application of principal component analysis
Weatherly, Choyce A., et al.
Journal of Chromatography. B, Biomedical Applications, 955-956, 72-80 (2014)
Nilusha L T Padivitage et al.
Drug testing and analysis, 6(6), 542-551 (2013-10-12)
Recently a novel class of chiral stationary phases (CSPs) based on cyclofructan (CF) has been developed. Cyclofructans are cyclic oligosaccharides that possess a crown ether core and pendent fructofuranose moieties. Herein, we evaluate the applicability of these novel CSPs for

Conteúdo relacionado

CYCLOBOND is the name given to Astec technology for bonding cyclodextrins to a high purity silica gel through a stable ether linkage.

Chromatograms

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