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Sigma-Aldrich

KitAlysis High-Throughput Miyaura Borylation Reaction Screening Kit-Pack of 2

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About This Item

Código UNSPSC:
12161600
NACRES:
NA.21

adequação da reação

reagent type: catalyst
core: palladium
reaction type: Miyaura Borylation Reaction

grupo funcional

phosphine

Descrição geral

The KitAlysis High-Throughput Miyaura Borylation Reaction Screening Kit enables chemists to quickly and efficiently screen reaction conditions for Pd catalyzed Miyaura borylation reactions. Quick identification of optimal conditions allows faster scale-up of the desired synthetic transformation. All required chemicals come pre-weighed for ease of use. A step-by-step user guide and experimental excel sheets are available for download to facilitate the process.

Aplicação

Step-by-step user guides and a downloadable experimental excel sheets are provided in the below hyperlinks.
Step-by-Step Guide for Miyaura Borylation Reaction Screening Kit
Downloadable Experiment excel sheets

Each kit contains 2 customizable screening sets that include the following components:

  • 6 x 4 pre-weighed catalysts in glass vials loaded with stir bars and topped with cap mat.
  • 4 x 4 mL reaction vials with pre-weighed KOAc
  • Bis(pinacolato)diboron (473294), tetrahydroxydiboron (754242), and pinacol (221171)
  • 1 (2 mL) ampule each of toluene, THF, n-butanol, DMA, MeOH, MeCN, ethylene glycol and DIPEA.
  • 1 NEW KitAlysis 24-Well Reaction Block Replacement Film.
  • 4 stir bars for substrate stock solution vials.
  • 1 internal standard.
Monitor reaction progress via TLC-MS by following this protocol

Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).

Características e benefícios

  • Designed and tested by synthetic chemists.
  • Easily run 24-microscale reactions in parallel.
  • 10 μmol reactions with 1 μmol catalyst, 3 equiv. base, 0.1 M concentration.
  • Customizable Excel Template for quick calculations and easy incorporation into electronic laboratory notebooks.

Informações legais

KitAlysis is a trademark of Sigma-Aldrich Co. LLC

Componentes do kit também disponíveis separadamente

Nº do produto
Descrição
SDS

  • 764175P(Cy3) Pd G3, 97%SDS

  • 791733Potassium acetate, anhydrous, free-flowing, Redi-Dri, ACS reagent, ≥99.0%SDS

  • 804274XPhos Pd G4, 95%SDS

  • 804282SPhos Pd G4SDS

  • 804290RuPhos Pd G4SDS

  • 804975DTBPF-Pd-G3SDS

  • 900349cataCXium Pd G4SDS

  • 900522Toluene, anhydrous, ZerO2®, 99.8%SDS

  • 900631Ethylene glycol, anhydrous, ZerO2®, 99.8%SDS

  • 900634N,N-Dimethylacetamide, anhydrous, ZerO2®, 99.8%SDS

  • 900636Tetrahydrofuran, anhydrous, inhibitor-free, ZerO2®, ≥99.9%SDS

  • 9006391-Butanol, anhydrous, ZerO2®, 99.8%SDS

  • 900641Methanol, anhydrous, ZerO2®, 99.8%SDS

  • 900644Acetonitrile, anhydrous, ZerO2®, 99.8%SDS

  • 900690N,N-Diisopropylethylamine, purified by redistillation, ZerO2®, 99.5%SDS

  • 221171Pinacol, 98%SDS

  • 473294Bis(pinacolato)diboron, 99%SDS

  • 754242Tetrahydroxydiboron, 95%SDS

  • B34656Biphenyl, ReagentPlus®, 99.5%SDS

  • Z118850Spinbar® magnetic stirring fleas, red, L 10 mm, diam. 3 mmSDS

  • Z742110KitAlysis 24-well reaction block replacement filmSDS

Ver tudo (21)

Palavra indicadora

Danger

Classificações de perigo

Acute Tox. 3 Dermal - Acute Tox. 3 Inhalation - Acute Tox. 3 Oral - Aquatic Acute 1 - Aquatic Chronic 1 - Carc. 2 - Eye Dam. 1 - Flam. Liq. 2 - Repr. 1B - Skin Irrit. 2 - STOT RE 2 Oral - STOT SE 1 - STOT SE 3

Órgãos-alvo

Central nervous system, Eyes,Central nervous system, Kidney, Respiratory system

Perigos de suplementos

Código de classe de armazenamento

3 - Flammable liquids

Ponto de fulgor (°F)

1.4 °F

Ponto de fulgor (°C)

-17 °C


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Artigos

KitAlysis High-Throughput Screening Kits provide solution to efficiently identify or optimize suitable catalytic reaction conditions. Chemist can rapidly run 24 unique micro scale reactions in parallel with tailored conditions.

Protocolos

Catalyst screening, KitAlysis™ High-Throughput Screening Kits, Thin layer chromatography (TLC), parallel analysis, parallel synthesisigh-Throughput Buchwald-Hartwig Amination Reaction Screening Kit, TLC-MS analysis

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Chemical reaction design and optimization in organic synthesis aims to precisely alter reaction parameters to achieve optimum results in finding pathways to target molecules.

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