Pular para o conteúdo
Merck
Todas as fotos(6)

Documentos Principais

KITALYSIS-CUCN

Sigma-Aldrich

KitAlysis High-Throughput Copper C-N Cross-Coupling Reaction Screening Kit-Pack of 2

Sinônimo(s):

Copper Catalyzed C-N Coupling Kit

Faça loginpara ver os preços organizacionais e de contrato


About This Item

Código UNSPSC:
12161503
NACRES:
NA.22

adequação da reação

core: palladium
reaction type: Buchwald-Hartwig Cross Coupling Reaction
reaction type: Heck Reaction
reaction type: Hiyama Coupling
reaction type: Negishi Coupling
reaction type: Sonogashira Coupling
reaction type: Stille Coupling
reaction type: Suzuki-Miyaura Coupling
reagent type: catalyst
reaction type: Cross Couplings

Aplicação

Screening kit for Copper C-N Cross-Coupling Reactions. Step-by-step user guides and a downloadable experimental excel sheets are provided in the below hyperlinks.

Step-by-Step Guide for KitAlysis High-Throughput Copper C-N Cross-Coupling Reaction Screening Kit

Downloadable experimental excel sheet

Each kit contains 2 customizable screening sets that include the following components:
  • 24 (6 x 4) pre-weighed ligands in glass vials loaded with stir bars, topped with cap mat
  • Potassium phosphate: 4 pre-weighed vials with product labels and lids
  • CuI (soluble source) in preweighed vial
  • 4 degassed anhydrous solvents (dioxane, DMAc, toluene, and DMSO) in ampules
  • 1 internal standard
  • 2 KitAlysis 24-Well reaction block replacement films
  • 8 stir bars for stock solutions
  • Ampule cracker

Monitor reaction progress via TLC-MS by following this protocol

Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).

Características e benefícios

  • Designed and tested by synthetic chemists.
  • Easily run 24-microscale reaction in parallel.
  • Suggested conditions: 10 μmol reactions with 1 μmol catalyst (10 mol%) 0.1 M concentration, and 3 equiv. base.
  • Customizable and downloadable Excel Template for quick calculations and easy incorporation into electronic laboratory notebooks.

Informações legais

KitAlysis is a trademark of Sigma-Aldrich Co. LLC

Palavra indicadora

Danger

Classificações de perigo

Acute Tox. 4 Dermal - Acute Tox. 4 Inhalation - Acute Tox. 4 Oral - Aquatic Acute 1 - Aquatic Chronic 1 - Asp. Tox. 1 - Carc. 1B - Eye Dam. 1 - Flam. Liq. 2 - Repr. 1B - Skin Irrit. 2 - STOT RE 2 Inhalation - STOT SE 3

Órgãos-alvo

Central nervous system, Respiratory system

Perigos de suplementos

Código de classe de armazenamento

3 - Flammable liquids

Ponto de fulgor (°F)

39.2 °F

Ponto de fulgor (°C)

4 °C


Escolha uma das versões mais recentes:

Certificados de análise (COA)

Lot/Batch Number

It looks like we've run into a problem, but you can still download Certificates of Analysis from our Documentos section.

Se precisar de ajuda, entre em contato Atendimento ao cliente

Já possui este produto?

Encontre a documentação dos produtos que você adquiriu recentemente na biblioteca de documentos.

Visite a Biblioteca de Documentos

Artigos

KitAlysis High-Throughput Screening Kits provide solution to efficiently identify or optimize suitable catalytic reaction conditions. Chemist can rapidly run 24 unique micro scale reactions in parallel with tailored conditions.

Materials included in your KITALYSIS-CUCN-2PK High-Throughput Screening Kit

Conteúdo relacionado

Chemical reaction design and optimization in organic synthesis aims to precisely alter reaction parameters to achieve optimum results in finding pathways to target molecules.

Nossa equipe de cientistas tem experiência em todas as áreas de pesquisa, incluindo Life Sciences, ciência de materiais, síntese química, cromatografia, química analítica e muitas outras.

Entre em contato com a assistência técnica