242403
(Bromomethyl)cyclopropane
97%
Sinônimo(s):
Cyclopropylmethyl bromide
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About This Item
Produtos recomendados
Nível de qualidade
Ensaio
97%
forma
liquid
índice de refração
n20/D 1.457 (lit.)
pb
105-107 °C (lit.)
densidade
1.392 g/mL at 25 °C (lit.)
cadeia de caracteres SMILES
BrCC1CC1
InChI
1S/C4H7Br/c5-3-4-1-2-4/h4H,1-3H2
chave InChI
AEILLAXRDHDKDY-UHFFFAOYSA-N
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Descrição geral
The coupling reaction of (bromomethyl)cyclopropane with phenylmagnesium bromide was studied.
Aplicação
(Bromomethyl)cyclopropane was used as a synthetic building block for the introduction of the cyclopropylmethyl group. It was also used in the synthesis of 1,4-dienes via iron-catalyzed cross-coupling with alkenyl Grignard reagents.
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Warning
Frases de perigo
Declarações de precaução
Classificações de perigo
Acute Tox. 4 Oral - Flam. Liq. 3
Código de classe de armazenamento
3 - Flammable liquids
Classe de risco de água (WGK)
WGK 3
Ponto de fulgor (°F)
105.8 °F
Ponto de fulgor (°C)
41 °C
Equipamento de proteção individual
Eyeshields, Faceshields, Gloves, type ABEK (EN14387) respirator filter
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Chemical communications (Cambridge, England), (33)(33), 4161-4163 (2005-08-16)
Mixtures of iron(III) chloride and appropriate amine ligands are active catalysts for the coupling of aryl Grignard reagents with primary and secondary alkyl halide substrates bearing beta-hydrogens, under mild and simple reaction conditions.
Journal of medicinal chemistry, 47(6), 1400-1412 (2004-03-05)
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Iron-catalyzed cross-coupling of alkyl halides with alkenyl grignard reagents.
Angewandte Chemie (International ed. in English), 46(34), 6521-6524 (2007-07-28)
Bioorganic & medicinal chemistry letters, 14(8), 1991-1995 (2004-03-31)
(S)-N-[1-(4-Cyclopropylmethyl-3,4-dihydro-2H-benzo[1,4]oxazin-6-yl)-ethyl]-3-(2-fluoro-phenyl)-acrylamide ((S)-2) was identified as a potent and efficacious KCNQ2 opener. This compound demonstrated significant activity in reducing neuronal hyperexcitability in rat hippocampal slices, and the inhibition mediated by (S)-2 was reversed by the KCNQ blocker linopirdine.
Bioorganic & medicinal chemistry letters, 14(2), 377-381 (2003-12-31)
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