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Analiza HPLC środków odurzających na urządzeniu 2445 Express F5

Analiza HPLC środków odurzających na urządzeniu 2445 Express F5 application for HPLC

Materiały

Standardowe

Numer produktu
Opis
Cennik

Codeine monohydrate

analytical standard

Morphine sulfate salt pentahydrate

analytical standard

Benzoylecgonine solution

100 μg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

Fentanyl solution

100 μg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

Hydrocodone solution

1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

(±)-MDMA solution

1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

(±)-Methamphetamine solution

100 μg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

Meperidine solution

1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

Normeperidine solution

100 μg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

(+)-Propoxyphene solution

1.0 mg/mL in acetonitrile, ampule of 1 mL, certified reference material, Cerilliant®

kolumna analityczna

Numer produktu
Opis
Cennik

Ascentis® Express HILIC, 2.7 μm HPLC Column

2.7 μm particle size, L × I.D. 7.5 cm × 3 mm

CONDITIONS

column

Ascentis Express F5, 10 cm x 2.1 mm I.D., 2.7 μm particles (53569-U)

mobile phase

[A] 5 mM ammonium formate; [B] 5 mM ammonium formate in 95:5 (v/v) acetonitrile:water

gradient

held at 20% B for 0.5 min; 20 to 100% B in 5.5 min; held at 100% B for 4 min

flow rate

0.3 mL/min

pressure

175 bar

column temp.

35 °C

detector

ESI(+), m/z 100-1000

injection

1 μL

sample

1 μg/mL in 50:50, water: methanol

Opis

Informacje prawne

Ascentis is a registered trademark of Merck KGaA, Darmstadt, Germany