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391484

Supelco

Silica gel

high-purity grade (7734), pore size 60 Å, 70-230 mesh

CAS Number:
EC Number:
MDL number:
PubChem Substance ID:
NACRES:
SB.52

grade

high-purity grade (7734)

Quality Level

form

powder

manufacturer/tradename

EMD Millipore®

technique(s)

LPLC: suitable

matrix

Silica

matrix active group

silica

particle size

63-200 μm
70-230 mesh

pore size

~0.8 cm3/g pore volume
60 Å

surface area

550 m2/g

bp

2230 °C

mp

>1600 °C

separation technique

hydrophilic interaction (HILIC)

SMILES string

O=[Si]=O

InChI

1S/O2Si/c1-3-2

InChI key

VYPSYNLAJGMNEJ-UHFFFAOYSA-N

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General description

Silica gel is a rigid 3D network of colloidal silica. It is exclusively used as a support material for the active titanium(III) centers in Ziegler-Natta catalysts. Silica gel allows a controlled fragmentation resulting in the formation of uniform polymer particles with narrow particle size distribution and high bulk density. Silica gel is classified as below:
a. Aquagel - pores are filled with water
b. Xerogel - by the process of evaporation, aqueous phase in the pores are removed
c. Aerogel - solvent removed by supercritical extraction

Application

Silica gel was used as an adsorbent to separate compounds by chromatography. It was used to compare MCM-41 type mesoporous adsorbents.
It may be used in the synthesis of the following:
  • Silica gel-immobilized-dithioacetal derivatives.
  • Piperazino silica reagent for removing 9-fluorenylmethyloxycarbonyl amino protecting group.
  • Polysiloxanes silica hybrids.

Packaging

100 g in poly bottle
5 kg in fiber drum
1 kg in poly bottle

Legal Information

EMD Millipore is a registered trademark of Merck KGaA, Darmstadt, Germany

Storage Class Code

11 - Combustible Solids

WGK

nwg

Flash Point(F)

Not applicable

Flash Point(C)

Not applicable

Certificate of Analysis

Enter Lot Number to search for Certificate of Analysis (COA).

Certificate of Origin

Enter Lot Number to search for Certificate of Origin (COO).

Nonlinear absorption properties of some 1, 4, 8, 11, 15, 18, 22, 25-octaalkylphthalocyanines and their metallated derivatives.
Auger A, et al.
Journal of Materials Chemistry, 13(5), 1042-1047 (2003)
Silica gel-immobilized-dithioacetal derivatives as potential solid phase extractors for mercury (II).
Mahmoud ME and Gohar GA.
Talanta, 51(1), 77-87 (2000)
Branched functionalised polysiloxane-silica hybrids for immobilisation of catalysts.
Rozga-Wijas, K, et al.
Journal of Materials Chemistry, 13(9), 2301-2310 (2003)
Piperazino-functionalized silica gel as a deblocking-scavenging agent for the 9-fluorenylmethyloxycarbonyl amino-protecting group.
Carpino LA, et al.
The Journal of Organic Chemistry, 48(5), 666-669 (1983)
T Martin et al.
Chemical communications (Cambridge, England), (1)(1), 24-25 (2002-07-18)
Texture-related features of water intrusion in hydrophobised MCM-41 silicas render these materials especially suitable for energy dissipation in mechanical dampers.

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