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HPLC Analysis of α-Methylbenzylamine Enantiomers (3,5-Dinitrobenzoyl Derivatives) on Astec® CHIROBIOTIC® V

HPLC Analysis of α-Methylbenzylamine Enantiomers (3,5-Dinitrobenzoyl Derivatives) on Astec® CHIROBIOTIC® V application for HPLC

Materials

analytical column

Product No.
Description
Pricing

Astec® CHIROBIOTIC® V Chiral HPLC Column

5 μm particle size, L × I.D. 25 cm × 4.6 mm

standard

Product No.
Description
Pricing

(S)-(−)-α-Methylbenzylamine

for chiral derivatization, LiChropur, ≥99.0%

(R)-(+)-α-Methylbenzylamine

for chiral derivatization, LiChropur, ≥99.0%

(R)-(+)-α-Methylbenzylamine

purum, ≥98.0% (sum of enantiomers, GC)

(R)-(+)-α-Methylbenzylamine

98%

(S)-(−)-α-Methylbenzylamine

98%

α-Methylbenzylamine

99%

CONDITIONS

column

CHIROBIOTIC V, 25 cm x 4.6 mm I.D., 5 μm particles (11024AST)

mobile phase

[A] hexane; [B] isopropanol; (90:10, A:B)

flow rate

0.5 mL/min

column temp.

25 °C

detector

UV, 254 nm

injection

1 μL

sample

2 mg/mL in methanol

Description

Legal Information

Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
CHIROBIOTIC is a registered trademark of Sigma-Aldrich Co. LLC