Analiza GC podstawowych leków na 3325-5ms(20 m x 0,18 mm I.D., 0,36 μm) po SPME przy użyciu włókna poliakrylanowego 85 μm, szybka analiza GC

sample/matrix

500 ug/L of each compound in 2 mL 0.05M phosphate buffer, pH=11, plus sodium chloride (NaCl) to 25% (w/v)

SPME fiber

85 μm Polyacrylate (57304)

extraction

immersion, 450 rpm stirring at room temp. for 15 min

desorption process

250 °C for 3 min

column

SLB-5ms, 20 m x 0.18 mm I.D. x 0.36 μm (28576-U)

oven

100 °C (1 min), 20 °C/min to 325 °C (5 min)

MSD interface

325 °C

carrier gas

helium, 1.5 mL/min. constant

liner

0.75 mm I.D. SPME