Analiza GC enancjomerów 5-amino-1,3,3-trimetylocykloheksanemetyloaminy (pochodnych N-TFA) na 6513 3836 B-TA
CONDITIONS
column
Astec CHIRALDEX B-TA, 30 m x 0.25 mm I.D., 0.12 μm (73023AST)
oven
160 °C
inj. temp.
250 °C
detector
FID, 250 °C
carrier gas
helium, 30 psi
injection
1 μL, 80:1 split
sample
3 mg/mL racemate in methanol
peaks 1 & 2: first enantiomer pair
peaks 3 & 4: second enantiomer pair
Opis
Informacje prawne
Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
CHIRALDEX is a trademark of Sigma-Aldrich Co. LLC