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Merck

55408-U

Supelco

Supel QuE QuEChERS tube

Z-Sep+ Tube, centrifuge tube volume 2 mL, pack of 100 ea

Synonim(y):

QuEChERS

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About This Item

Kod UNSPSC:
41115712
NACRES:
NB.21

product name

Supel QuE, Z-Sep+ Tube, centrifuge tube volume 2 mL, pack of 100 ea

Materiały

polypropylene tube

Poziom jakości

linia produktu

Supel

skład

Z-Sep+, 75 mg

opakowanie

pack of 100 ea

metody

QuEChERS: suitable

pojemność probówki reakcyjnej (do wirowania)

2 mL

grupa aktywna macierzy

zirconia-based phase

Zastosowanie

food and beverages

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Opis ogólny

Dispersive SPE (dSPE), often referred to as the "QuEChERS" method (Quick, Easy, Cheap, Effective, Rugged, and Safe), is modern sample prep technique that is becoming increasingly popular in the area of multi-residue pesticide analysis in food and agricultural products.

Using the QuEChERS method, food/agricultural samples are first extracted with an aqueous miscible solvent (e.g., acetonitrile) in the presence of high amounts of salts (e.g., sodium chloride and magnesium sulfate) and/or buffering agents (e.g. citrate) to induce liquid phase separation and stabilize acid and base labile pesticides, respectively. Upon shaking and centrifugation, an aliquot of the organic phase is subjected to further cleanup using SPE. Unlike traditional methods using SPE tubes, in dispersive SPE, cleanup is facilitated by mixing bulk amounts of SPE (e.g., Supelclean PSA, ENVI-Carb, and/or Discovery DSC-18) with the extract. After sample cleanup, the mixture is centrifuged and the resulting supernatant can either be analyzed directly or can be subjected to minor further treatment before analysis.

Supelco carries a line of vials and centrifuge tubes containing pre-determined amounts of salts and SPE sorbents to support the most common method configurations used today.

Inne uwagi

Supel QuE Z-Sep products enhance sample cleanup for complex matrices by effectively removing more fat and color from sample extracts than traditional phases for QuEChERS methods. By eliminating problematic matrix interferences, Z-Sep products provide more robust LC-MS and GC-MS methods. This proprietary technology can replace C18 and PSA in your current methods without additional method development.

Z-Sep+ is recommended for cleanup of samples containing greater than 15% fat.
Z-Sep/C18 is recommended for cleanup of samples containing less than 15% fat.
Z-Sep is recommended for cleanup of samples prior to analysis of hydrophobic analytes.

Informacje prawne

Certain uses of this product may be covered by the claims of one or more pending patent applications. For licensing inquiries please contact techserv@sial.com
AOAC is a registered trademark of AOAC International
Supel is a trademark of Sigma-Aldrich Co. LLC
This page may contain text that has been machine translated.

Kod klasy składowania

11 - Combustible Solids

Klasa zagrożenia wodnego (WGK)

nwg

Temperatura zapłonu (°F)

Not applicable

Temperatura zapłonu (°C)

Not applicable


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Journal of chromatography. A, 1343, 69-78 (2014-04-22)
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Journal of chromatography. A, 1339, 34-41 (2014-03-25)
A Quick, Easy, Cheap, Effective, Rugged and Safe (QuEChERS) extraction method followed by liquid chromatography-(Orbitrap) high resolution mass spectrometry was developed for the simultaneous determination of five benzotriazole, four benzothiazole and five benzenesulfonamide derivates in sewage sludge. While the method

Protokoły

A short abstract on a method using QuEChERS and GC/MS/MS for determination of fipronil & fipronil sulfone.

broad spectrum insecticide, egradation product, phenylpyrazole pesticide, World Health Organization (WHO), HPLC, UV, testing of Fipronil and Fipronil sulfone in Food

LC/MS/MS Analysis of Pesticide Residues in Pistachios on the Ascentis® Express RP-Amide Column after QuEChERS Extraction

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