GCによるアミノ酸 (TBDMS 誘導体) の分析、SLB^®-5ms [Fast GC Analysis]

column

SLB-5ms, 20 m × 0.18 mm I.D., 0.18 μm (28564-U)

oven

100 °C (1 min), 35 °C/min to 290 °C (3 min), 40 °C/min to 360 °C

inj. temp.

250 °C

MSD interface

325 °C

scan range

m/z = 40-450

carrier gas

helium, 1 mL/min, constant

injection

0.5 μL, splitless (1.0 min)

liner

2 mm I.D., straight

sample

TBDMS derivatives of amino acids, each approximately 23 ug/mL