おすすめの製品
品質水準
製品種目
Novabiochem®
アッセイ
≥98% (TLC)
≥98.0% (HPLC)
形状
powder
反応適合性
reaction type: Boc solid-phase peptide synthesis
メーカー/製品名
Novabiochem®
アプリケーション
peptide synthesis
保管温度
15-25°C
InChI
1S/C18H23N3O6S/c1-12-5-7-14(8-6-12)28(25,26)21-10-13(19-11-21)9-15(16(22)23)20-17(24)27-18(2,3)4/h5-8,10-11,15H,9H2,1-4H3,(H,20,24)(H,22,23)/t15-/m0/s1
InChI Key
DCLJSEPKYJSEHW-HNNXBMFYSA-N
関連するカテゴリー
詳細
Standard building block for introduction of histidine amino-acid residues by Boc SPPS.
Associated Protocols and Technical Articles
Cleavage and Deprotection Protocols for Boc SPPS
Literature references
[1] T. Fujii, et al. (1974) Bull. Chem. Soc. Jpn., 47, 3146.
[2] J. M. v. d. Eijk, et al. (1980) J. Org. Chem., 45, 547.
Associated Protocols and Technical Articles
Cleavage and Deprotection Protocols for Boc SPPS
Literature references
[1] T. Fujii, et al. (1974) Bull. Chem. Soc. Jpn., 47, 3146.
[2] J. M. v. d. Eijk, et al. (1980) J. Org. Chem., 45, 547.
関連事項
Replaces: 04-12-0012
アナリシスノート
Colour (visual): white to slight yellow to beige
Appearance of substance (visual): powder
Identity (IR): passes test
Optical rotation α 25/D (c=1 in dioxan): +10.0 - +13.0 °
Purity (TLC(011B)): ≥ 98 %
Purity (TLC(011C)): ≥ 98 %
Assay (HPLC, area%): ≥ 98.0 % (a/a)
Solubility (50 mg in ml EtOH): clearly soluble
To see the solvent systems used for TLC of Novabiochem® products please click here.
Appearance of substance (visual): powder
Identity (IR): passes test
Optical rotation α 25/D (c=1 in dioxan): +10.0 - +13.0 °
Purity (TLC(011B)): ≥ 98 %
Purity (TLC(011C)): ≥ 98 %
Assay (HPLC, area%): ≥ 98.0 % (a/a)
Solubility (50 mg in ml EtOH): clearly soluble
To see the solvent systems used for TLC of Novabiochem® products please click here.
法的情報
Novabiochem is a registered trademark of Merck KGaA, Darmstadt, Germany
保管分類コード
11 - Combustible Solids
WGK
WGK 3
引火点(°F)
Not applicable
引火点(℃)
Not applicable
試験成績書(COA)
製品のロット番号・バッチ番号を入力して、試験成績書(COA) を検索できます。ロット番号・バッチ番号は、製品ラベルに「Lot」または「Batch」に続いて記載されています。
プロトコル
The most popular reagent for cleavage of peptides from Boc-based resins is anhydrous HF. Of all the cleavage procedures HF appears to be the most versatile and least harmful to a wide variety of peptides synthesized on Boc-based resins.
ライフサイエンス、有機合成、材料科学、クロマトグラフィー、分析など、あらゆる分野の研究に経験のあるメンバーがおります。.
製品に関するお問い合わせはこちら(テクニカルサービス)