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Merck
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Key Documents

Altri documenti

23184

Sigma-Aldrich

Fmoc cloruro

BioReagent, ≥99.0% (HPLC)

Sinonimo/i:

9-fluorenilmetil cloroformiato, 9-fluorenilmetilossicarbonil cloruro, Fmoc-Cl

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About This Item

Formula empirica (notazione di Hill):
C15H11ClO2
Numero CAS:
28920-43-6
Peso molecolare:
258.70
Beilstein:
2279177
Numero CE:
249-313-6
Numero MDL:
MFCD00001138
Codice UNSPSC:
12352200
ID PubChem:
329752391

Nome Commerciale

BioReagent

Livello qualitativo

100

Saggio

≥99.0% (HPLC)

Forma fisica

solid

Punto di fusione

61-64 °C
62-64 °C (lit.)

Gruppo funzionale

Fmoc

Temperatura di conservazione

2-8°C

Stringa SMILE

ClC(=O)OCC1c2ccccc2-c3ccccc13

InChI

1S/C15H11ClO2/c16-15(17)18-9-14-12-7-3-1-5-10(12)11-6-2-4-8-13(11)14/h1-8,14H,9H2
IRXSLJNXXZKURP-UHFFFAOYSA-N

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Categorie correlate

Applicazioni

9-Fluorenylmethoxycarbonyl chloride (Fmoc-Cl) is a reagent for pre-column derivatization of amino acids and biogenic amines for HPLC amino acid analysis and for preparing N-Fmoc amino acids for solid-phase peptide synthesis.
Reagente per la derivatizzazione di aminoacidi per l′analisi degli aminoacidi con HPLC e per la preparazione di aminoacidi N-Fmoc per la sintesi peptidica in fase solida.

Altre note

Reagent for the pre-column fluorescent derivatization of amino acids

Pittogrammi

Corrosion
GHS05

Avvertenze

Danger

Indicazioni di pericolo

H314

Classi di pericolo

Eye Dam. 1 - Skin Corr. 1B

Rischi supp

EUH029

Codice della classe di stoccaggio

8A - Combustible, corrosive hazardous materials

Classe di pericolosità dell'acqua (WGK)

WGK 3

Punto d’infiammabilità (°F)

Not applicable

Punto d’infiammabilità (°C)

Not applicable

Dispositivi di protezione individuale

Eyeshields, Faceshields, Gloves, type P3 (EN 143) respirator cartridges

Certificati d'analisi (COA)

Cerca il Certificati d'analisi (COA) digitando il numero di lotto/batch corrispondente. I numeri di lotto o di batch sono stampati sull'etichetta dei prodotti dopo la parola ‘Lotto’ o ‘Batch’.

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3-Ferrocenylpropionic anhydride for HPLC derivatization, LiChropur™, ≥98.0% (C)

Supelco

76737

3-Ferrocenylpropionic anhydride

1,8-Diazafluoren-9-one

Sigma-Aldrich

33484

1,8-Diazafluoren-9-one

Ftaldialdeide suitable for HPLC fluorimetric detection of amino acids, ≥99% (HPLC), powder or crystals

Sigma-Aldrich

P0657

Ftaldialdeide

Valentin Lozanov et al.
Journal of chromatography. B, Analytical technologies in the biomedical and life sciences, 860(1), 92-97 (2007-11-07)
A liquid chromatography method for simultaneous analysis of amino acids, polyamines, catecholeamines and metanephrines in human body fluids after derivatization with 9-fluorenylmethyloxycarbonyl chloride was developed. The chromatographic behavior of analytes at different pH of mobile phase was studied. Successful baseline
Ibolya Molnár-Perl
Journal of chromatography. B, Analytical technologies in the biomedical and life sciences, 879(17-18), 1241-1269 (2011-03-05)
An overview is presented on the advancement of the two most frequently used derivatization protocols applying the o-phthalaldehyde (OPA)-thiol and the fluorenylmethyloxycarbonyl (FMOC) chloride reagents, prior to the high performance liquid chromatographic analysis of amino acids. This review pays special
E J Miller et al.
Analytical biochemistry, 190(1), 92-97 (1990-10-01)
A recently described procedure for amino acid analyses has been modified and adapted for use in quantitating the unique mixture of products commonly found in hydrolysates of the collagens. The method involves precolumn derivatization of hydrolysates with 9-fluorenylmethyl chloroformate (FMOC-CL)
A Jámbor et al.
Journal of chromatography. A, 1216(34), 6218-6223 (2009-07-28)
This paper, as a novelty to this field, presents the deproteinization and derivatization of plasma's free amino acids (PFAAs), simultaneously, in a single step, with the acetonitrile (ACN) containing 9-fluorenylmethyloxycarbonyl chloride (FMOC) reagent. Deproteinization and derivatization, were studied with 22
P Fürst et al.
Journal of chromatography, 499, 557-569 (1990-01-19)
Reversed-phase high-performance liquid chromatography (RP-HPLC) is a powerful method for assaying physiological amino acid concentrations in biological fluids. Four pre-column derivatization methods, with o-phthaldialdehyde (OPA), 9-fluorenylmethyl chloroformate (FMOC-Cl), phenyl isothiocyanate (PITC) and 1-dimethylaminonaphthalene-5-sulphonyl chloride (dansyl-Cl), were assessed with respect to
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