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US EPA Method 8082: GC Analysis of Aroclor 1016/1260 (PCBs) on SLB®-5ms

US EPA Method 8082: GC Analysis of Aroclor 1016/1260 (PCBs) on SLB®-5ms suitable for GC

Materiais

Padrão

Nº do produto
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Aroclor 1232 solution

certified reference material, 1000 μg/mL in isooctane

Aroclor 1242 solution

certified reference material, 1000 μg/mL in isooctane

Aroclor 1248 solution

certified reference material, 1000 μg/mL in isooctane

Aroclor 1254 solution

certified reference material, 1000 μg/mL in isooctane

Aroclor 1260 solution

certified reference material, 1000 μg/mL in isooctane

Aroclor 1262 solution

certified reference material, 1000 μg/mL in isooctane

Aroclor 1221 solution

certified reference material, 1000 μg/mL in isooctane

Aroclor 1254 solution

certified reference material, 200 μg/mL in methanol

Aroclor Standard Mix 1

certified reference material, in acetone: methanol (2:3) (varied)

Aroclor 1016 solution

certified reference material, 1000 μg/mL in isooctane

Pesticide Surrogate Spike Mix

certified reference material, TraceCERT®, 200 μg/mL each component in acetone, ampule of 1 mL

acessório

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Wheaton wide-mouth bottle

amber soda-lime glass bottle, capacity 1000 mL, white polypropylene cap, (PTFE faced LDPE liner), case of 12 ea

coluna analítica

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SPB®-608 Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 0.25 μm

SPB®-608 Capillary GC Column

L × I.D. 30 m × 0.53 mm, df 0.50

Equity-1701 Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 0.25 μm

Equity-1701 Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 1.00 μm

Equity-1701 Capillary GC Column

L × I.D. 30 m × 0.53 mm, df 0.50 μm

Coluna de GC capilar SLB®-5ms

L × I.D. 30 m × 0.25 mm, df 0.25 μm

Coluna de GC capilar SLB®-5ms

L × I.D. 30 m × 0.25 mm, df 1.00 μm

Coluna de GC capilar SLB®-5ms

L × I.D. 15 m × 0.10 mm, df 0.10 μm

necessário, mas não fornecido

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"Y" GlasSeal Connector, Borosilicate Glass

pkg of 1 ea

"Y" GlasSeal Connector, Fused Silica

pkg of 1 ea

"Y" GlasSeal Connector, Fused Silica

pkg of 3 ea

pré-coluna

Nº do produto
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Preços

Non-Polar Fused Silica Tubing

L × I.D. 5.0 m × 0.10 mm

Non-Polar Fused Silica Tubing

L × I.D. 5.0 m × 0.25 mm

Non-Polar Fused Silica Tubing

L × I.D. 5.0 m × 0.53 mm

recomendado

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Polyimide Sealing Resin

pkg of 5 g

CONDITIONS

column

SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)

oven

100 °C (2 min), 15 °C/min to 330 °C (3 min)

inj. temp.

250 °C

detector

ECD, 330 °C

carrier gas

helium, 25 cm/sec, constant

injection

2 μL splitless (0.75 min)

liner

4 mm I.D., single taper

sample

Aroclor standard mix 1 (46846-U) diluted to 500 ppb / 50 ppb (Aroclors / surrogates) in n-hexane

Descrição

Nota de análise

Aroclors are commercial mixtures of PCB congeners. Due to their stability, they ave been used in many different industrial and commercial applications. Because of their toxicity and ability to bioaccumulate, production of these materials ceased in 1977. This application demonstrates the separation of two common Aroclor mixtures, Aroclor 1016 and Aroclor 1260 on the SLB-5ms.

Informações legais

SLB is a registered trademark of Merck KGaA, Darmstadt, Germany