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86853

Supelco

Bissulfato de tetrabutilamônio

suitable for ion pair chromatography, LiChropur™, ≥99.0%

Sinônimo(s):

Hidrogenossulfato de tetrabutilamônio

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About This Item

Fórmula linear:
(CH3CH2CH2CH2)4N(HSO4)
Número CAS:
32503-27-8
Peso molecular:
339.53
Beilstein:
3599663
Número CE:
251-068-5
Número MDL:
MFCD00011637
Código UNSPSC:
12000000
ID de substância PubChem:
329769496
NACRES:
NB.21
Ensaio:
≥99.0% (T)
≥99.0%
Formulário:
crystals

descrição

cationic

Nível de qualidade

100

Ensaio

≥99.0% (T)
≥99.0%

Formulário

crystals

qualidade

LiChropur™

técnica(s)

ion pair chromatography: suitable

pf

171-174 °C

traços de ânion

bromide (Br-): ≤50 mg/kg

λ

10 % in H2O

Absorção UV

λ: 210 nm Amax: 0.06
λ: 220 nm Amax: 0.05
λ: 230 nm Amax: 0.03
λ: 260 nm Amax: 0.02
λ: 500 nm Amax: 0.02

adequação

corresponds to standard for RP gradient test
corresponds to standard for filter test

cadeia de caracteres SMILES

OS([O-])(=O)=O.CCCC[N+](CCCC)(CCCC)CCCC

InChI

1S/C16H36N.H2O4S/c1-5-9-13-17(14-10-6-2,15-11-7-3)16-12-8-4;1-5(2,3)4/h5-16H2,1-4H3;(H2,1,2,3,4)/q+1;/p-1

chave InChI

SHFJWMWCIHQNCP-UHFFFAOYSA-M

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Descrição geral

Tetrabutyammonium bisulfate (TBAHS) is an ion-pairing reagent. It acts as a catalyst in hydrolysis of aziridines and epoxides and the catalyst can be recycled.

Aplicação

TBAHS was suitable as ion-pairing reagent in determination and separation of thallium using ionic liquid-assisted ion-pairing liquid-liquid microextraction and inductively coupled plasma mass spectrometry. It was suitable as mobile phase component for a HPLC-UV analysis to quantify chondroitin sulfate.

Informações legais

LiChropur is a trademark of Merck KGaA, Darmstadt, Germany

Pictogramas

CorrosionExclamation mark
GHS05,GHS07

Palavra indicadora

Danger

Frases de perigo

H302,H314,H412

Classificações de perigo

Acute Tox. 4 Oral - Aquatic Chronic 3 - Eye Dam. 1 - Skin Corr. 1

Código de classe de armazenamento

8A - Combustible corrosive hazardous materials

Classe de risco de água (WGK)

WGK 2

Ponto de fulgor (°F)

348.1 °F - closed cup

Ponto de fulgor (°C)

175.6 °C - closed cup

Equipamento de proteção individual

dust mask type N95 (US), Eyeshields, Gloves

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Certificados de análise (COA)

Lot/Batch Number
BCCG9547
BCCF4498
BCCD5969
BCCC5073
BCCB7504

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Supelco

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Tetrabutylammonium chloride

Leticia B Escudero et al.
Journal of hazardous materials, 244-245, 380-386 (2012-12-29)
A fast and simple method involving separation and determination of thallium (Tl) species, based on novel ionic liquid-assisted ion pairing dispersive liquid-liquid microextraction (DLLME) method, was developed. Initially, Tl(III) was selectively complexed with chloride ion to form [TlCl(4)](-) chlorocomplex. Subsequently
David Ji et al.
Journal of AOAC International, 90(3), 659-669 (2007-06-22)
A method to quantify chondroitin sulfate in raw materials and dietary supplements at a range of about 5 to 100% (w/w) chondroitin sulfate has been developed and validated. The chondroitin sulfate is first selectively hydrolyzed by chondroitinase ACII enzyme to
Ren-Hua Fan et al.
Organic & biomolecular chemistry, 1(9), 1565-1567 (2003-08-21)
Bu4NHSO4 (TBAHS) is an effective catalyst for the hydrolysis of aziridines and epoxides under mild and non-metal conditions to give the corresponding beta-amino alcohols and 1,2-diols in high yields. The catalyst can be recycled.
K M Frankowski et al.
Journal of dairy science, 97(9), 5356-5370 (2014-07-16)
Many food companies are trying to limit the amount of sodium in their products. Permeate, the liquid remaining after whey or milk is ultrafiltered, has been suggested as a salt substitute. The objective of this study was to determine the
R Bryan Sears et al.
Journal of inorganic biochemistry, 121, 77-87 (2013-01-29)
The complex cis-[Ru(phpy)(phen)(CH3CN)2](+) (phpy=2-phenylpyridine, phen=1,10-phenanthroline) was investigated as a potential photodynamic therapy (PDT) agent. This complex presents desirable photochemical characteristics including a low energy absorption tail extending into the PDT window (600-850nm) and photoinduced exchange of the CH3CN ligands, generating
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Protocolos

Analysis of Difficult Polar Compounds using Sigma-Aldrich Ion Pair Reagents and Supelco Ascentis HPLC Columns

Because reversed-phase HPLC is primarily dependent on hydrophobic interactions between the stationary phase and analyte, ion pairing is occasionally necessary to obtain sufficient retention of polar, ionizable compounds.

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