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US EPA Method 8082: GC Analysis of Aroclor 1016/1260 (PCBs) on SLB®-5ms

US EPA Method 8082: GC Analysis of Aroclor 1016/1260 (PCBs) on SLB®-5ms suitable for GC

Materialien

Analytische Säule

Produkt-Nr.
Beschreibung
Preisangaben

24103-U

SPB®-608 Kapillar-GC-Säule

L × I.D. 30 m × 0.25 mm, df 0.25 μm

25312

SPB®-608 Kapillar-GC-Säule

L × I.D. 30 m × 0.53 mm, df 0.50

28372-U

Equity-1701 Kapillar-GC-Säule

L × I.D. 30 m × 0.25 mm, df 0.25 μm

28378-U

Equity-1701 Kapillar-GC-Säule

L × I.D. 30 m × 0.25 mm, df 1.00 μm

28391-U

Equity-1701 Kapillar-GC-Säule

L × I.D. 30 m × 0.53 mm, df 0.50 μm

28471-U

SLB®-5ms GC-Kapillarsäule

L × I.D. 30 m × 0.25 mm, df 0.25 μm

28476-U

SLB®-5ms GC-Kapillarsäule

L × I.D. 30 m × 0.25 mm, df 1.00 μm

28466-U

SLB®-5ms GC-Kapillarsäule

L × I.D. 15 m × 0.10 mm, df 0.10 μm

Empfehlung

Produkt-Nr.
Beschreibung
Preisangaben

23817

Polyimid-Dichtungsharz

pkg of 5 g

Erforderlich, aber nicht bereitgestellt

Produkt-Nr.
Beschreibung
Preisangaben

20480

"Y" GlasSeal Connector, Borosilicate Glass

pkg of 1 ea

23631

„Y“-förmiger GlasSeal-Verbinder, Quarzglas

pkg of 1 ea

23632

„Y“-förmiger GlasSeal-Verbinder, Quarzglas

pkg of 3 ea

Standard

Produkt-Nr.
Beschreibung
Preisangaben

44805

Aroclor 1232 -Lösung

certified reference material, 1000 μg/mL in isooctane

44806

Aroclor 1242 -Lösung

certified reference material, 1000 μg/mL in isooctane

44807

Aroclor 1248 -Lösung

certified reference material, 1000 μg/mL in isooctane

44808

Aroclor 1254 -Lösung

certified reference material, 1000 μg/mL in isooctane

44809

Aroclor 1260 -Lösung

certified reference material, 1000 μg/mL in isooctane

44810

Aroclor 1262 -Lösung

certified reference material, 1000 μg/mL in isooctane

48098

Aroclor 1221 -Lösung

certified reference material, 1000 μg/mL in isooctane

48707

Aroclor 1254 -Lösung

certified reference material, 200 μg/mL in methanol

46846-U

Aroclor Standardmischung 1

certified reference material, in acetone: methanol (2:3) (varied)

48097

Aroclor 1016 -Lösung

certified reference material, 1000 μg/mL in isooctane

CRM48460

Pestizid-Surrogat-Spike-Mischung

certified reference material, TraceCERT®, 200 μg/mL each component in acetone, ampule of 1 mL

Vorsäule

Produkt-Nr.
Beschreibung
Preisangaben

25740-U

Nichtpolare Quarzglasröhrchen

L × I.D. 5.0 m × 0.10 mm

25742

Nichtpolare Quarzglasröhrchen

L × I.D. 5.0 m × 0.25 mm

25744

Nichtpolare Quarzglasröhrchen

L × I.D. 5.0 m × 0.53 mm

Zubehör

Produkt-Nr.
Beschreibung
Preisangaben

Z250228

Wheaton Weithalsflasche

amber soda-lime glass bottle, capacity 1000 mL, white polypropylene cap, (PTFE faced LDPE liner), case of 12 ea

CONDITIONS

column

SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)

oven

100 °C (2 min), 15 °C/min to 330 °C (3 min)

inj. temp.

250 °C

detector

ECD, 330 °C

carrier gas

helium, 25 cm/sec, constant

injection

2 μL splitless (0.75 min)

liner

4 mm I.D., single taper

sample

Aroclor standard mix 1 (46846-U) diluted to 500 ppb / 50 ppb (Aroclors / surrogates) in n-hexane

Beschreibung

Hinweis zur Analyse

Aroclors are commercial mixtures of PCB congeners. Due to their stability, they ave been used in many different industrial and commercial applications. Because of their toxicity and ability to bioaccumulate, production of these materials ceased in 1977. This application demonstrates the separation of two common Aroclor mixtures, Aroclor 1016 and Aroclor 1260 on the SLB-5ms.

Rechtliche Hinweise

SLB is a registered trademark of Merck KGaA, Darmstadt, Germany

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