GC Analysis of Total Petroleum Hydrocarbons (TPH) on SLB^®-5ms (20 m x 0.18 mm I.D., 0.18 μm), Fast GC Analysis

column

SLB-5ms, 20 m x 0.18 mm I.D., 0.18 μm (28564-U)

oven

70 °C (0.5 min), 20 °C/min to 360 °C (1 min)

inj. temp.

275 °C

detector

FID, 365 °C

carrier gas

hydrogen, 2.5 mL/min constant

injection

0.50 μL, 200:1 split

liner

2 mm I.D. straight

sample

TPH Mix 3, each analyte at 1000 μg/mL in carbon disulfide (861394-U)