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GC Analysis of Amphetamine and Methamphetamine Enantiomers (N-Trifluoroacetyl Derivatives) on Astec® CHIRALDEX™ G-PN

GC Analysis of Amphetamine and Methamphetamine Enantiomers (N-Trifluoroacetyl Derivatives) on Astec® CHIRALDEX™ G-PN suitable for GC

Materials

Analytical column

Product No.
Description
Pricing

74033AST

Astec® CHIRALDEX™ G-PN Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 0.12 μm

Standard

Product No.
Description
Pricing

M8750

(+)-Methamphetamine hydrochloride

A219

DL-Amphetamine-d6 hydrochloride

100 μg/mL in methanol

A3278

D-Amphetamine hemisulfate salt solution

1.0 mg/mL in methanol, analytical standard, for drug analysis

M5260

(+)-Methamphetamine hydrochloride solution

analytical standard, for drug analysis, 1.0 mg/mL in methanol

A1263

DL-Amphetamine sulfate salt

A5880

D-Amphetamine hemisulfate salt

A218

DL-Amphetamine-d6 solution

0.1 mg/mL in methanol

CONDITIONS

column

Astec CHIRALDEX G-PN, 30 m x 0.25 mm I.D., 0.12 μm (74033AST)

oven

130 °C

detector

FID, 250 °C

inj. temp.

250 °C

carrier gas

helium, 30 psi

injection

1 μL, 80:1 split

sample

3 mg/mL each compound in methanol
peak 1: d-methamphetamine
peak 2: l-methamphetamine
peak 3: l-amphetamine
peak 4: d-amphetamine

Description

Analysis Note

Elution order reversal of amphetamine (d,l) by using CHIRALDEX G-DP, 140°C.

Legal Information

Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
CHIRALDEX is a trademark of Sigma-Aldrich Co. LLC

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