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52688-U

Supelco

Discovery® DSC-SCX SPE Tube

bed wt. 500 mg, volume 6 mL, pk of 30

Synonym(s):

Strong Cation Exchange SPE cartridge tube

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About This Item

UNSPSC Code:
41115712
NACRES:
NB.21

material

polypropylene tube

composition

bed wt., 500 mg

packaging

pk of 30

technique(s)

solid phase extraction (SPE): suitable

surface area

480 m2/g

volume

6 mL

matrix

Silica gel base material (irregularly shaped, acid washed)

matrix active group

sulfonic acid bonding

particle size

50 μm

pore size

0.9 mL/g pore volume
70 Å pore diameter

capacity

0.8 meq/g total capacity

application(s)

food and beverages

separation technique

ion exchange

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General description

Retention Mechanism: Cation exchange
Sample Matrix Compatibility: Organic or aqueous solutions

  • A polymerically bonded, benzene sulfonic acid functional group, pKa (< 1.0)
  • Counter ion is H+
  • Silica support allows for use with very organic solvents (no shrinking/swelling)
  • Excellent capacity (0.8 meq/g) for cleaning up solution phase combinatorial chemistry reactions (removing target molecules from reaction by-products and excess reagents)
  • The presence of the benzene ring offers some mixed-mode capabilities (hydrophobic interactions) that should be considered when extracting cations from aqueous matrices

Legal Information

Discovery is a registered trademark of Merck KGaA, Darmstadt, Germany

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Danger

Hazard Classifications

Aquatic Chronic 2 - Eye Dam. 1 - Flam. Sol. 1 - Skin Corr. 1A - Skin Sens. 1

Storage Class

4.1B - Flammable solid hazardous materials

wgk_germany

WGK 3

flash_point_f

Not applicable

flash_point_c

Not applicable

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Certificates of Analysis (COA)

Lot/Batch Number
15035701
11207101
10866601
10584801
9902301

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52604-U

Discovery® DSC-18 SPE Tube

Articles

Solid Phase Extraction: Ion Exchange Methodology

SPE retention mechanism in this case is based on the electrostatic attraction of charged functional groups of the analyte(s) to oppositely charged functional groups on the sorbent.

Protocols

Analysis of Melamine in Milk

Melamine was extracted from milk using Supelco® Discovery® DSC-SCX SPE tubes. Analysis was performed by HPLC, using an Ascentis® Express HILIC column.

Solid Phase Extraction: Normal Phase Methodology

Retention occurs through polar interaction between the sorbent and analytes. Typical sample matrices that can be employed in normal-phase SPE include hydrocarbon or fatty oils diluted in a solvent like hexane, isooctane, chlorinated solvent, THF, diethyl ether, or ethyl acetate.

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