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46385

Supelco

Florisil® Adsorbent for Chromatography

60-100 mesh

Synonym(s):
Magnesium silicate, Florisil®, Activated magnesium silicate
Empirical Formula (Hill Notation):
MgO3Si
CAS Number:
Molecular Weight:
100.39
EC Number:
MDL number:
PubChem Substance ID:
NACRES:
SB.52

Quality Level

grade

standard

form

coarse powder

application(s)

LPLC: suitable

matrix

Magnesium silicate hydrate

matrix active group

magnesium silicate hydrate

particle size

149-250 μm
60-100 mesh

pore size

60 Å mean pore size

surface area

289 m2/g

separation technique

hydrophilic interaction (HILIC)

SMILES string

[Mg++].[O-][Si]([O-])=O

InChI

1S/Mg.O3Si/c;1-4(2)3/q+2;-2

InChI key

FKHIFSZMMVMEQY-UHFFFAOYSA-N

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General description

Florisil, adsorbent for the separation of lipids, is a commercially-prepared magnesia silica gel. It has a coarse mesh size which helps in rapid flow rate. Florisil is effective in promoting [1,3]-sigmatropic shift of myceophenolic acid related allyl phenyl ethers. Florisil cartridges are used in atmospheric sampling to assess possible interference from air contaminants.

Application

Florisil was used:
  • as column packing material in column chromatography
  • as an adsorbent in gas chromatography with electron capture detector (GC/ECD), capillary column chromatography, adsorption column chromatography
  • in clean-up procedures in gas chromatography-tandem mass spectrometry and GC-FID

Caution

may contain some dark particles

Legal Information

Florisil is a registered trademark of U.S. Silica Company

Storage Class Code

13 - Non Combustible Solids

WGK

nwg

Flash Point(F)

Not applicable

Flash Point(C)

Not applicable

Personal Protective Equipment

dust mask type N95 (US),Eyeshields,Gloves

Certificate of Analysis

Certificate of Origin

An improved gas chromatographic method for the determination of perfluorocarbon tracers in the atmosphere
Lagomarsino, Raymond J.
Journal of Chromatography A, 34, 405-412 (1996)
R C Prados-Rosales et al.
Journal of chromatography. A, 993(1-2), 121-129 (2003-05-09)
A rapid analytical method for determination of organochlorine pesticide residues in sunflower seeds based on focused microwave-assisted Soxhlet extraction has been developed. The main factors affecting the extraction efficiency--namely microwave power, irradiation time, volume of extractant and number of cycles--were...
Determination of atmospheric perfluorocarbon background concentrations of fL/L range at the western coastal area of Korea
Kim, HyeKyeong, et al.
Atmospheric Environment, 1, 4-4 (2002)
The covalently bound flavin of Chromatium cytochrome c552. 1. Evidence for cysteine thiohemiacetal at the 8 alpha position.
W H Walker et al.
European journal of biochemistry, 48(2), 439-448 (1974-10-02)
Andrew C Singer et al.
Environmental toxicology and chemistry, 22(9), 1998-2004 (2003-09-10)
This study investigated the interactive effects of bioaugmentation, biostimulation, and the rhizosphere during remediation of Aroclor 1242-contaminated soil. Treatments were repeatedly augmented with polychlorinated bipheny (PCB)-degrading bacteria, inducers (carvone and salicylic acid), surfactant (sorbitan trioleate), minimal salts medium in a...

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