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GC Analysis of 1-Methoxy-2-Propylamine Enantiomers (N-Chloroacetyl Derivatives) on Astec® CHIRALDEX B-PH

GC Analysis of 1-Methoxy-2-Propylamine Enantiomers (N-Chloroacetyl Derivatives) on Astec® CHIRALDEX™ B-PH suitable for GC

Materials

analytical column

Product No.
Description
Pricing

Astec® CHIRALDEX B-PH Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 0.12 μm

Standard

Product No.
Description
Pricing

1-Methoxy-2-propylamine

95%

(S)-1-Methoxy-2-propylamine

ChiPros®, produced by BASF, 99%

CONDITIONS

column

Astec CHIRALDEX B-PH, 30 m x 0.25 mm I.D., 0.12 μm (71023AST)

oven

120 °C

inj. temp.

250 °C

detector

FID, 250 °C

carrier gas

helium, 24 psi

injection

1 μL, 80:1 split

sample

3 mg/mL in methanol
peaks 1 & 2: 1-methoxy-2-propylamine enantiomers (N-chloroacetyl derivatives)

Description

Legal Information

Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
CHIRALDEX is a trademark of Sigma-Aldrich Co. LLC