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주요 문서

KITALYSIS-24PD

Sigma-Aldrich

KitAlysis High-Throughput 24 Pd Precatalyst Reaction Screening Kit-Pack of 2

동의어(들):

Pd Precatalysts

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About This Item

UNSPSC 코드:
12161600
NACRES:
NA.22

반응 적합성

reaction type: Buchwald-Hartwig Cross Coupling Reaction
reaction type: Heck Reaction
reaction type: Hiyama Coupling
reaction type: Negishi Coupling
reaction type: Sonogashira Coupling
reaction type: Stille Coupling
reaction type: Suzuki-Miyaura Coupling
reagent type: catalyst
reaction type: Cross Couplings

작용기

phosphine

애플리케이션

Screening kit for cross-coupling reactions. Step-by-step user guides and a downloadable experimental excel sheets are provided in the below hyperlinks.
Step-by-Step Guide for KitAlysis High-Throughput Palladium Precatalyst Cross-Coupling Reaction Screening Kit

Downloadable experimental Excel Sheet

Each kit contains 2 customizable screening sets that include the following components:

  • 24 pre-weighed catalysts in glass micro vials loaded with stir bars and topped with cap mat.
  • 2 KitAlysis 24-Well reaction block replacement films.
  • 4 empty substrate stock solution reaction vials with stir bars.
  • 3 stir bars for stock solutions.
  • 1 internal standard.

Monitor reaction progress via TLC-MS by following this protocol

Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).

특징 및 장점

  • Designed and tested by synthetic chemists.
  • Easily run 24-microscale reaction in parallel.
  • Suggested conditions: 10 μmol reactions with 1 μmol catalyst (10 mol%) 0.1 M concentration, and 3 equiv. base.
  • Customizable and downloadable excel template for quick calculations and easy incorporation into electronic laboratory notebooks.

법적 정보

KitAlysis is a trademark of Sigma-Aldrich Co. LLC

픽토그램

Health hazardExclamation markEnvironment

신호어

Warning

Hazard Classifications

Acute Tox. 4 Dermal - Acute Tox. 4 Inhalation - Acute Tox. 4 Oral - Aquatic Acute 1 - Aquatic Chronic 1 - Carc. 2 - Eye Irrit. 2 - Skin Irrit. 2 - Skin Sens. 1 - STOT SE 3

표적 기관

Central nervous system, Respiratory system

보충제 위험성

Storage Class Code

10 - Combustible liquids

Flash Point (°F)

Not applicable

Flash Point (°C)

Not applicable


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시험 성적서(COA)

Lot/Batch Number

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문서 라이브러리 방문

문서

Materials Included in your KITALYSIS-24PD-2PK High-Throughput Screening Kit

Materials Included in your KITALYSIS-24PD-2PK High-Throughput Screening Kit

프로토콜

Catalyst screening, KitAlysis™ High-Throughput Screening Kits, Thin layer chromatography (TLC), parallel analysis, parallel synthesisigh-Throughput Buchwald-Hartwig Amination Reaction Screening Kit, TLC-MS analysis

관련 콘텐츠

Chemical reaction design and optimization in organic synthesis aims to precisely alter reaction parameters to achieve optimum results in finding pathways to target molecules.

자사의 과학자팀은 생명 과학, 재료 과학, 화학 합성, 크로마토그래피, 분석 및 기타 많은 영역을 포함한 모든 과학 분야에 경험이 있습니다..

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