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Merck

KITALYSIS-PHO

Sigma-Aldrich

KitAlysis High-Throughput 24-Catalyst Photoredox Reaction Screening Kit-Pack of 2

Sinónimos:

high-throughput photoredox catalyst screening kit

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About This Item

Código UNSPSC:
12352300
NACRES:
NA.22

idoneidad de la reacción

reagent type: catalyst
reaction type: Photocatalysis

Aplicación

Screening kit for photocatalytic reactions to be used with Photo KitAlysis Starter Kit. Step-by-step user guide is provided in the below hyperlink.
Step-by-Step Guide for Photocatalysis Reaction Screening Kit
Downloadable experimental excel file

Each kit contains 2 customizable screening sets that include the following components:
  • 24 pre-weighed catalysts in glass vials loaded with stir bars and topped with cap mat
  • 4 degassed anhydrous solvents (DCM, DCE, DMF, MeCN)
  • 1 NEW KitAlysis 24-Well Reaction Block Replacement Film
  • 4 empty substrate stock solution reaction vials with stirbars
  • 1 internal standard

For use Photo KitAlysis High-Throughput Screen Platform (sold seperately)Monitor reaction progress via TLC-MS by following this protocol

Best when used with KitAlysis Benchtop Inertion Box (sold separately).

Features:
  • Designed and tested by synthetic chemists
  • Easily run 24-microscale reactions in parallel
  • 10 μmol reactions with 1 μmol catalyst, 0.1 M concentration
  • Customizable Excel Template for quick calculations and easy incorporation into electronic laboratory notebooks

Información legal

KitAlysis is a trademark of Sigma-Aldrich Co. LLC

Los componentes del kit también están disponibles por separado

Referencia del producto
Descripción
SDS

  • 224758Tris(2,2′-bipyridyl)dichlororuthenium(II) hexahydrate, powderSDS

  • 232017Tetrachloro-1,4-benzoquinone, 99%SDS

  • 2723452,4,6-Triphenylpyrylium tetrafluoroborate, 98%SDS

  • 318337Acridine Orange hydrochloride hydrate, ≥98% (HPLC)SDS

  • 333190Bismuth(III) sulfide, 99%SDS

  • 343714Dichlorotris(1,10-phenanthroline)ruthenium(II) hydrate, 98%SDS

  • 4598529,10-Anthracenedicarbonitrile, 97%SDS

  • 46955Fluorescein, for fluorescence, free acidSDS

  • 637017Bismuth(III) oxide, nanopowder, 90-210 nm particle size, 99.8% trace metals basisSDS

  • 688096Tris[2-phenylpyridinato-C2,N]iridium(III), 97%SDS

  • 747769[Ir(dtbbpy)(ppy)2]PF6SDS

  • 747777[Ru(bpz)3][PF6]2, 95%SDS

  • 747785[Ru(bpm)3][Cl]2SDS

  • 747793(Ir[dF(CF3)ppy]2(dtbpy))PF6SDS

  • 7932219-Mesityl-10-phenylacridinium tetrafluoroborateSDS

  • 7938769-Mesityl-2,7-dimethyl-10-phenylacridinium tetrafluoroborateSDS

  • 7941719-Mesityl-10-methylacridinium tetrafluoroborateSDS

  • 804215[Ir{dFCF3ppy}2(bpy)]PF6SDS

  • 9004219-Mesityl-3,6-di-tert-butyl-10-phenylacridinium tetrafluoroborate, ≥95%SDS

  • 9006922,4,6-Tris(4-methoxyphenyl)pyrylium tetrafluoroborateSDS

  • 9006939-Mesityl-1,3,6,8-tetramethoxy-10-phenylacridin-10-ium tetrafluoroborate, 95%SDS

  • 90069410-(3,5-Dimethoxyphenyl)-9-mesityl-1,3,6,8-tetramethoxyacridin-10-ium tetrafluoroborate, ≥93%SDS

  • D604002,3-Dichloro-5,6-dicyano-p-benzoquinone, 98%SDS

  • P2508Proflavine hemisulfate salt hydrate, powderSDS

  • 900633Dichloromethane, anhydrous, contains 40-150 ppm amylene as stabilizer, ZerO2®, ≥99.8%SDS

  • 9006371,2-Dichloroethane, anhydrous, ZerO2®, 99.8%SDS

  • 900638N,N-Dimethylformamide, anhydrous, ZerO2®, 99.8%SDS

  • 900644Acetonitrile, anhydrous, ZerO2®, 99.8%SDS

  • B34656Biphenyl, ReagentPlus®, 99.5%SDS

  • Z118850Spinbar® magnetic stirring fleas, red, L 10 mm, diam. 3 mmSDS

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Referencia del producto
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Palabra de señalización

Danger

Clasificaciones de peligro

Acute Tox. 3 Inhalation - Acute Tox. 3 Oral - Acute Tox. 4 Dermal - Aquatic Acute 1 - Aquatic Chronic 1 - Asp. Tox. 1 - Carc. 1B - Eye Dam. 1 - Flam. Liq. 2 - Muta. 2 - Repr. 1B - Skin Irrit. 2 - Skin Sens. 1 - STOT RE 2 Oral

Órganos de actuación

Kidney

Riesgos supl.

Código de clase de almacenamiento

3 - Flammable liquids

Clase de riesgo para el agua (WGK)

WGK 3

Punto de inflamabilidad (°F)

35.6 °F - closed cup

Punto de inflamabilidad (°C)

2.0 °C - closed cup


Certificados de análisis (COA)

Busque Certificados de análisis (COA) introduciendo el número de lote del producto. Los números de lote se encuentran en la etiqueta del producto después de las palabras «Lot» o «Batch»

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Artículos

The PhotoKitAlysis Reaction Kit was designed to provide the best possible chance of finding good reaction conditions for cross-coupling reactions: pre-weighed base or base solution (provided), 10–20 mmol coupling partner (user supplied), 10 mmol aryl halide substrate (user supplied), Catalysts (user supplied), 6 solvents (toluene, DMA. THJF, n-butanol, MeOH, MeCN) (provided).

Protocolos

The Photo KitAlysis Photoreactor Controller allows you maximum control of photocatalysis reactions.

Materials and procedure Step-by-Step Guide for Photocatalysis High-Throughput Reaction Screening Kit

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