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Key Documents

20724AST

Supelco

Astec® CYCLOBOND I 2000 DMP Chiral (5 μm) HPLC Columns

L × I.D. 25 cm × 4.6 mm, HPLC Column

Sinonimo/i:

TM=["CYCLOBOND"] I 2000 DMP Chiral HPLC Column

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About This Item

Codice UNSPSC:
41115700
eCl@ss:
32110501
NACRES:
SB.52

product name

Astec® Cyclobond I 2000 DMP Chiral HPLC Column, 5 μm particle size, L × I.D. 25 cm × 4.6 mm

Materiali

stainless steel column

Nome Commerciale

Astec®

Confezionamento

pkg of 1 ea

Produttore/marchio commerciale

Astec®

Parametri

0-50 °C temperature
172 bar pressure (2500 psi)

tecniche

HPLC: suitable
LC/MS: suitable

Lungh. × D.I.

25 cm × 4.6 mm

Matrice

silica particle platform
fully porous particle

Gruppo funzionale matrice

cyclodextrin, beta- phase

Dimensione particelle

5 μm

Dimensione pori

100 Å

pH di lavoro

3.5-7

Tecnica di separazione

chiral

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Descrizione generale

The reaction of the 3,5-dimethylphenyl isocyanate with the hydroxyl groups of β-cyclodextrin results in a pi-basic phase similar in character to the naphthylethyl carbamate phases. The selectivity is greater for the CYCLOBOND I 2000 DMP when the chiral center of the analyte is part of a ring structure or is on the α carbon. This phase has been very useful for derivatized amines, like amphetamine ACQ.

  • Bonded phase: 3,5-Dimethylphenyl carbamate modified β-cyclodextrin

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Note legali

Astec is a registered trademark of Merck KGaA, Darmstadt, Germany

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Indirect photodetection of pregnanolone on a Cyclobond column by high-performance liquid chromatography
Agnus, Benoit, et al.
Journal of Chromatography A, 633 (1), 27-33 (1994)
Rapid high-performance liquid chromatographic separation of barley malt a-amylase on cyclobond columns
Henson, Cynthia A., Stone, Julie M.
Journal of Chromatography A, 469, 361-367 (1989)
Reprint of: Enantiomeric separation of functionalized ethano-bridged Troger bases using macrocyclic cyclofructan and cyclodextrin chiral selectors in high-performance liquid chromatography and capillary electrophoresis with application of principal component analysis
Weatherly, Choyce A., et al.
Journal of Chromatography. B, Biomedical Applications, 968, 40-48 (2014)
Enantiomeric separation of functionalized ethano-bridged Troger bases using macrocyclic cyclofructan and cyclodextrin chiral selectors in high-performance liquid chromatography and capillary electrophoresis with application of principal component analysis
Weatherly, Choyce A., et al.
Journal of Chromatography. B, Biomedical Applications, 955-956, 72-80 (2014)
Nilusha L T Padivitage et al.
Drug testing and analysis, 6(6), 542-551 (2013-10-12)
Recently a novel class of chiral stationary phases (CSPs) based on cyclofructan (CF) has been developed. Cyclofructans are cyclic oligosaccharides that possess a crown ether core and pendent fructofuranose moieties. Herein, we evaluate the applicability of these novel CSPs for

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