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Sigma-Aldrich

KitAlysis High-Throughput 24-Catalyst Photoredox Reaction Screening Kit-Pack of 2

Synonym(e):

high-throughput photoredox catalyst screening kit

Anmeldenzur Ansicht organisationsspezifischer und vertraglich vereinbarter Preise


About This Item

UNSPSC-Code:
12161600
NACRES:
NA.22

Eignung der Reaktion

reagent type: catalyst
reaction type: Photocatalysis

Anwendung

Screening kit for photocatalytic reactions to be used with Photo KitAlysis Starter Kit. Step-by-step user guide is provided in the below hyperlink.
Step-by-Step Guide for Photocatalysis Reaction Screening Kit
Downloadable experimental excel file

Each kit contains 2 customizable screening sets that include the following components:
  • 24 pre-weighed catalysts in glass vials loaded with stir bars and topped with cap mat
  • 4 degassed anhydrous solvents (DCM, DCE, DMF, MeCN)
  • 1 NEW KitAlysis 24-Well Reaction Block Replacement Film
  • 4 empty substrate stock solution reaction vials with stirbars
  • 1 internal standard

For use Photo KitAlysis High-Throughput Screen Platform (sold seperately)Monitor reaction progress via TLC-MS by following this protocol

Best when used with KitAlysis Benchtop Inertion Box (sold separately).

Features:
  • Designed and tested by synthetic chemists
  • Easily run 24-microscale reactions in parallel
  • 10 μmol reactions with 1 μmol catalyst, 0.1 M concentration
  • Customizable Excel Template for quick calculations and easy incorporation into electronic laboratory notebooks

Rechtliche Hinweise

KitAlysis is a trademark of Sigma-Aldrich Co. LLC

Kit-Komponenten auch einzeln erhältlich

Produkt-Nr.
Beschreibung
SDB

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  • 232017Tetrachloro-1,4-benzoquinone, 99%SDB

  • 2723452,4,6-Triphenylpyrylium tetrafluoroborate, 98%SDB

  • 318337Acridine Orange hydrochloride hydrate, ≥98% (HPLC)SDB

  • 333190Bismuth(III) sulfide, 99%SDB

  • 343714Dichlorotris(1,10-phenanthroline)ruthenium(II) hydrate, 98%SDB

  • 4598529,10-Anthracenedicarbonitrile, 97%SDB

  • 46955Fluorescein, for fluorescence, free acidSDB

  • 637017Bismuth(III) oxide, nanopowder, 90-210 nm particle size, 99.8% trace metals basisSDB

  • 688096Tris[2-phenylpyridinato-C2,N]iridium(III), 97%SDB

  • 747769[Ir(dtbbpy)(ppy)2]PF6SDB

  • 747777[Ru(bpz)3][PF6]2, 95%SDB

  • 747785[Ru(bpm)3][Cl]2SDB

  • 747793(Ir[dF(CF3)ppy]2(dtbpy))PF6SDB

  • 7932219-Mesityl-10-phenylacridinium tetrafluoroborateSDB

  • 7938769-Mesityl-2,7-dimethyl-10-phenylacridinium tetrafluoroborateSDB

  • 7941719-Mesityl-10-methylacridinium tetrafluoroborateSDB

  • 804215[Ir{dFCF3ppy}2(bpy)]PF6SDB

  • 9004219-Mesityl-3,6-di-tert-butyl-10-phenylacridinium tetrafluoroborate, ≥95%SDB

  • 9006922,4,6-Tris(4-methoxyphenyl)pyrylium tetrafluoroborateSDB

  • 9006939-Mesityl-1,3,6,8-tetramethoxy-10-phenylacridin-10-ium tetrafluoroborate, 95%SDB

  • 90069410-(3,5-Dimethoxyphenyl)-9-mesityl-1,3,6,8-tetramethoxyacridin-10-ium tetrafluoroborate, ≥93%SDB

  • D604002,3-Dichloro-5,6-dicyano-p-benzoquinone, 98%SDB

  • P2508Proflavine hemisulfate salt hydrate, powderSDB

  • 900633Dichloromethane, anhydrous, contains 40-150 ppm amylene as stabilizer, ZerO2®, ≥99.8%SDB

  • 9006371,2-Dichloroethane, anhydrous, ZerO2®, 99.8%SDB

  • 900638N,N-Dimethylformamide, anhydrous, ZerO2®, 99.8%SDB

  • 900644Acetonitrile, anhydrous, ZerO2®, 99.8%SDB

  • B34656Biphenyl, ReagentPlus®, 99.5%SDB

  • Z118850Spinbar® magnetic stirring fleas, red, L 10 mm, diam. 3 mmSDB

Alle anzeigen (30)

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Signalwort

Danger

Gefahreneinstufungen

Acute Tox. 3 Inhalation - Acute Tox. 3 Oral - Acute Tox. 4 Dermal - Aquatic Acute 1 - Aquatic Chronic 1 - Asp. Tox. 1 - Carc. 1B - Eye Dam. 1 - Flam. Liq. 2 - Muta. 2 - Repr. 1B - Skin Irrit. 2 - Skin Sens. 1 - STOT RE 2 Oral - STOT SE 3

Zielorgane

Central nervous system, Kidney, Respiratory system

Zusätzliche Gefahrenhinweise

Lagerklassenschlüssel

3 - Flammable liquids

WGK

WGK 3

Flammpunkt (°F)

35.6 °F - closed cup

Flammpunkt (°C)

2.0 °C - closed cup


Hier finden Sie alle aktuellen Versionen:

Analysenzertifikate (COA)

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Artikel

The Photo KitAlysis Photoreactor Controller allows you maximum control of photocatalysis reactions.

The PhotoKitAlysis Reaction Kit was designed to provide the best possible chance of finding good reaction conditions for cross-coupling reactions: pre-weighed base or base solution (provided), 10–20 mmol coupling partner (user supplied), 10 mmol aryl halide substrate (user supplied), Catalysts (user supplied), 6 solvents (toluene, DMA. THJF, n-butanol, MeOH, MeCN) (provided).

Protokolle

Materials and procedure Step-by-Step Guide for Photocatalysis High-Throughput Reaction Screening Kit

Unser Team von Wissenschaftlern verfügt über Erfahrung in allen Forschungsbereichen einschließlich Life Science, Materialwissenschaften, chemischer Synthese, Chromatographie, Analytik und vielen mehr..

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