KITALYSIS-SM

KitAlysis^™ High-Throughput Suzuki-Miyaura Cross-Coupling Reaction Screening Kit - Pack of 4

• Synonym(e): Suzuki-Miyaura Cross-Coupling
• UNSPSC-Code: 12161600
• NACRES: NA.22

Eigenschaften

• Eignung der Reaktion: reaction type: Cross Couplings; reaction type: Suzuki-Miyaura Coupling; reagent type: catalyst; core: palladium
• Funktionelle Gruppe: phosphine

Beschreibung

Anwendung

Screening kit for Suzuki-Miyaura cross-coupling reaction. Step-by-step user guide and a downloadable experimental excel sheets are provided in the below hyperlink.
Step-by-Step Guide for Suzuki-Miyaura Cross-Coupling Reaction Screening Kit
Downloadable experimental excel sheet

Each kit contains 4 customizable screening sets that include the following components:

• 6 x 4 pre-weighed catalysts in glass vials loaded with stir bars and topped with cap mat.
• 1 (2 mL) ampule each of Toluene, THF, n-Butanol, DMAc, and aq. 1.5 M K₃PO_4.
• 4 NEW KitAlysis 24-Well Reaction Block Replacement Films.
• 4 substrate reaction vials with stir bars.
• 1 internal standard.

Monitor reaction progress via TLC-MS by following this protocol

Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).

Leistungsmerkmale und Vorteile

• Designed and tested by synthetic chemists.
• Easily run 24-microscale reactions in parallel.
• 10 μmol reactions with 1 μmol catalyst, 3 equiv. base, 0.1 M concentration.
• Customizable Excel Template for quick calculations and easy incorporation into electronic laboratory notebooks.

Rechtliche Hinweise

KitAlysis is a trademark of Sigma-Aldrich Co. LLC

Nur Kit-Komponenten

• SnapIT Ampule Opener, Regular, for 1-2ml, 5-10ml, 10-15ml ampoules 1 EA

Kit-Komponenten auch einzeln erhältlich

• 732117 Pd-PEPPSI^™-IPent catalyst, ≥95% 5 µmol
• 753009 SPhos Pd G2 5 µmol
• 761311 cataCXium^® A Pd G2 5 µmol
• 763381 XPhos Pd G3, 98%, 1:1 MTBE adduct 5 µmol
• 764175 P(Cy₃) Pd G3, 97% 5 µmol
• 764183 APhos Pd G3, 97% 5 µmol
• 900522 Toluene, anhydrous, ZerO₂^®, 99.8% 8 mL
900636 Tetrahydrofuran, anhydrous, inhibitor-free, ZerO₂^®, ≥99.9% 8 mL
900639 1-Butanol, anhydrous, ZerO₂^®, 99.8% 8 mL
900634 N,N-Dimethylacetamide, anhydrous, ZerO₂^®, 99.8% 8 mL
Degassed Potassium phosphate tribasic solution 8 mL
Z118850 Spinbar^® magnetic stirring fleas, red, L 10 mm, diam. 3 mm 1 EA

Alle anzeigen (12)

Sicherheitshinweise

• Piktogramme: GHS02,GHS08,GHS05,GHS07,GHS09
• Signalwort: Danger
• H-Sätze: H225,H302 + H312 + H332,H304,H315,H318,H335,H336,H351,H360D,H373,H410
• P-Sätze: P210 - P273 - P280 - P301 + P310 - P305 + P351 + P338 - P331
• Gefahreneinstufungen: Acute Tox. 4 Dermal - Acute Tox. 4 Inhalation - Acute Tox. 4 Oral - Aquatic Acute 1 - Aquatic Chronic 1 - Asp. Tox. 1 - Carc. 2 - Eye Dam. 1 - Flam. Liq. 2 - Repr. 1B - Skin Irrit. 2 - STOT RE 2 - STOT SE 3
• Zielorgane: Central nervous system, Respiratory system
• Zusätzliche Gefahrenhinweise: EUH019
• Lagerklassenschlüssel: 3 - Flammable liquids
• Flammpunkt (°F): 1.4 °F
• Flammpunkt (°C): -17 °C