LC/MS (TOF) Analysis of Opioids and Opiate-Dependence Management Drugs on Ascentis® Express HILIC
Materialien
Komponente der mobilen Phase
Produkt-Nr.
Beschreibung
Preisangaben
Standard
Produkt-Nr.
Beschreibung
Preisangaben
6-Acetylmorphin, 1,0 mg/ml -Lösung
1 mg/mL in acetonitrile, ampule of 1 mL, certified reference material, Cerilliant®Hydromorphon -Lösung
1 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®6-Acetylcodein -Lösung
1.0 mg/mL in acetonitrile, ampule of 1 mL, certified reference material, Cerilliant®Hydrocodon -Lösung
1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®Morphin -Lösung
1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®Oxycodon -Lösung
1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®CONDITIONS
column
Ascentis Express HILIC, 5 cm x 2.1 mm I.D., 2.7 μm particles (53934-U)
mobile phase
2 mM ammonium formate in 90:10 (v:v) acetonitrile:water
flow rate
0.3 mL/min
column temp.
55 °C
detector
TOF/MS
injection
2 μL
sample
400 ng/mL in acetonitrile
Beschreibung
Hinweis zur Analyse
The rapid analysis by HPLC with TOF-MS detection of seven opioids is shown here using an Ascentis Express HILIC column. Cerilliant CRMs were used to ensure reliable MS identification and quantification.
Rechtliche Hinweise
Ascentis is a registered trademark of Merck KGaA, Darmstadt, Germany