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23258

Sigma-Aldrich

2,2,2-Trichloroethyl chloroformate

purum, ≥98.0% (NT)

Sinónimos:

2,2,2-Trichloroethoxycarbonyl chloride

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About This Item

Fórmula lineal:
ClCOOCH2CCl3
Número de CAS:
17341-93-4
Peso molecular:
211.86
Beilstein/REAXYS Number:
970619
EC Number:
241-363-7
MDL number:
MFCD00000810
UNSPSC Code:
12352100
PubChem Substance ID:
329752403
NACRES:
NA.22

vapor pressure

0.06 psi ( 20 °C)

Quality Level

200

grade

purum

assay

≥98.0% (NT)

refractive index

n20/D 1.471 (lit.)
n20/D 1.471

bp

171-172 °C (lit.)

density

1.539 g/mL at 25 °C (lit.)

storage temp.

2-8°C

SMILES string

ClC(=O)OCC(Cl)(Cl)Cl

InChI

1S/C3H2Cl4O2/c4-2(8)9-1-3(5,6)7/h1H2

InChI key

LJCZNYWLQZZIOS-UHFFFAOYSA-N

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Application

2,2,2-Trichloroethyl chloroformate was used as:
  • derivatizing reagent in gas chromatographic/mass spectrometric determination of a large range of amphetamine-related drugs and ephedrines in plasma, urine and hair samples
  • starting reagent during the synthesis of 6-nor-9,10-dihydrolysergic acid methyl ester (IV)
  • reagent during N-demethylation of dextromethorphan
  • protecting group reagent for amines and alcohols

pictograms

Skull and crossbonesCorrosion
GHS06,GHS05

signalword

Danger

hcodes

H314,H331

Hazard Classifications

Acute Tox. 3 Inhalation - Eye Dam. 1 - Skin Corr. 1B

Storage Class

6.1A - Combustible acute toxic Cat. 1 and 2 / very toxic hazardous materials

wgk_germany

WGK 3

flash_point_f

Not applicable

flash_point_c

Not applicable

ppe

Faceshields, Gloves, Goggles, type ABEK (EN14387) respirator filter

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Certificados de análisis (COA)

Lot/Batch Number
BCCF3814
BCCC2921
BCCB6437
BCBW7361
BCBV8480

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X.S. He et al.
Synthetic Communications, 20, 2177-2177 (1990)
F. Farina et al.
Tetrahedron Letters, 32, 1109-1109 (1991)
M. Imoto et al.
Bulletin of the Chemical Society of Japan, 60, 2205-2205 (1987)
A Dasgupta et al.
Therapeutic drug monitoring, 20(3), 313-318 (1998-06-19)
Mexiletine (Mexitil) is an antiarrhythmic agent used in the treatment of ventricular arrhythmia. The drug has a narrow therapeutic window, and monitoring its serum concentration is recommended. The authors describe a gas chromatography-mass spectrometric (GC/MS) assay of mexiletine using selected
Giampietro Frison et al.
Rapid communications in mass spectrometry : RCM, 19(7), 919-927 (2005-03-05)
A new analytical approach, based on derivatization with 2,2,2-trichloroethyl chloroformate and gas chromatography/mass spectrometry (GC/MS), was investigated for qualitative and quantitative analyses of a large range of amphetamine-related drugs and ephedrines in plasma, urine and hair samples. Sample preparation involved
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