G006165

LC/MS Analysis of Fluoroamphetamine Drugs of Abuse on Ascentis^® Express HILIC

application for HPLC

特性

• テクニック: HPLC: suitable
• 試験パラメータ: column: Ascentis Express HILIC, 10 cm x 2.1 mm I.D., 2.7 μm particles (53939-U); gradient: 5 mM ammonium formate in acetonitrile:water (90:10, v/v); flow rate: 0.4 mL/min; column temp.: 35 °C; detector: TOF/MS; injection: 2 μL; sample: 300 ng/mL in acetonitrile
• 適合性: application for HPLC
• アプリケーション: forensics and toxicology

詳細

アナリシスノート

The fluoroamphetamines (FA) are a group of "designer" stimulant drugs in amphetamine family. The rapid LC/MS analysis of four members of the FA family on Ascentis Express HILIC is shown here. Cerilliant CRMs were used to ensure reliable MS identification and quantification.

法的情報

Ascentis is a registered trademark of Merck KGaA, Darmstadt, Germany

アナライト

(±)-2-Fluoroamphetamine hydrochloride solution, 1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant^®
4-Fluoroamphetamine hydrochloride solution, 1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant^®
(±)-2-Fluoromethamphetamine hydrochloride solution, 1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant^®
(±)-4-Fluoromethamphetamine hydrochloride solution, 1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant^®