US EPA Method 8100: GC Analysis of Polynuclear Aromatic Hydrocarbons (PAHs) on SPB^®-608

column

SPB-608, 30 m x 0.25 mm I.D., 0.25 μm (24103-U)

oven

80 °C (2 min), 15 °C/min to 250 °C, 8 °C/min to 300 °C (35 min)

inj. temp.

300 °C

MSD interface

300 °C

scan range

m/z 40 - 450

carrier gas

helium, 1.2 mL/min. constant

injection

0.5 μL, splitless (1 min)

sample

each analyte at 10 μg/mL in methylene chloride