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714836

Sigma-Aldrich

Iodine monochloride solution

1 M in acetic acid

Sinonimo/i:

Chloroiodide solution, Wijs solution

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About This Item

Formula condensata:
ICl
Numero CAS:
7790-99-0
Peso molecolare:
162.36
Beilstein:
3587194
Numero MDL:
MFCD00011354
Codice UNSPSC:
12352101
ID PubChem:
329763318
NACRES:
NA.22

Forma fisica

solution

Concentrazione

1 M in acetic acid

Densità

1.143 g/mL at 25 °C

Stringa SMILE

ClI

InChI

1S/ClI/c1-2
QZRGKCOWNLSUDK-UHFFFAOYSA-N

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Descrizione generale

Iodine monochloride is an inorganic reagent used in the iodination and chloroiodination of aromatic and unsaturated compounds, respectively. It is also used to cleave carbon-metal bonds.

Applicazioni

Iodine monochloride can be used:
  • As a reagent in the preparation of α-iodo β-ketosulfones from β-ketosulfones.
  • In the synthesis of 3-(4-bromo-2-methylphenyl)-4-iodosydnone, which is further used to prepare substituted pyrazoles.

Pittogrammi

FlameCorrosion
GHS02,GHS05

Avvertenze

Danger

Indicazioni di pericolo

H226,H314

Classi di pericolo

Eye Dam. 1 - Flam. Liq. 3 - Skin Corr. 1B

Codice della classe di stoccaggio

3 - Flammable liquids

Classe di pericolosità dell'acqua (WGK)

WGK 3

Punto d’infiammabilità (°F)

105.1 °F

Punto d’infiammabilità (°C)

40.6 °C

Certificati d'analisi (COA)

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Synthesis of α-iodo β-ketosulfones and α-iodo methylsulfones using iodine monochloride
Suryakiran N, et al.
Tetrahedron Letters, 47(26), 4319-4323 (2006)
R G Nielsen et al.
Journal of chromatography, 423, 41-50 (1987-12-25)
Low-level adsorption on the stationary phase has been studied using immunochemical reagents. An immunoaffinity column has been evaluated using affinity-purified radioisotope-labeled monoclonal antibodies. Recovery experiments including continuous immunosorbent monitoring have been performed. Proper characterization of an immunoaffinity separation can result
A Gafni
Biochimica et biophysica acta, 742(1), 91-99 (1983-01-12)
Rat muscle glyceraldehyde-3-phosphate dehydrogenase was reacted with two reagents aimed at the highly reactive cysteine-149 residue in the active site of the enzyme. The enzyme was rapidly inactivated by iodine monochloride. Complete inactivation occurred when approx. 6 mol ICl were
Zan Qu et al.
Journal of hazardous materials, 183(1-3), 132-137 (2010-08-03)
The removal of Hg(0) by the homogenous gas-phase reaction and particle-induced reaction was investigated under various conditions. Iodine monochloride was found to be efficient for Hg(0) oxidation, with the apparent 2nd-order rate constant of about 10.5(±0.3)×10(-17) cm(3) molecules(-1) s(-1) and
K R Siebenlist et al.
Biochemistry, 39(46), 14171-14175 (2000-11-23)
There are conflicting ideas regarding the location of the carboxyl-terminal regions of cross-linked gamma-chain dimers in double-stranded fibrin fibrils. Some investigators believe that the chains are always oriented longitudinally along each fibril strand and traverse the contacting ends of abutting
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