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M-108

Supelco

MTBSTFA

with 1% t-BDMCS, ampule of 5 × 1 mL, analytical standard, Cerilliant®

Sinónimos:

N-tert-Butyldimethylsilyl-N-methyltrifluoroacetamide with 1% tert-Butyldimethylchlorosilane, N-Methyl-N-tert-butyldimethylsilyltrifluoroacetamide, MTBSTFA + 1% TBDMSCl, Silylating mixture VI

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About This Item

Fórmula empírica (notación de Hill):
C9H18F3NOSi
Número de CAS:
77377-52-7
Peso molecular:
241.33
Beilstein:
3606546
Número MDL:
MFCD00009671
Código UNSPSC:
41116107
ID de la sustancia en PubChem:
329817850

Nombre del producto

N-tert-Butyldimethylsilyl-N-methyltrifluoroacetamide with 1% tert-Butyldimethylchlorosilane, (with 1% t-BDMCS), ampule of 5 × 1 mL, analytical standard, Cerilliant®

grado

analytical standard

Nivel de calidad

100

idoneidad de la reacción

reagent type: derivatization reagent
reaction type: Acylations

envase

ampule of 5 × 1 mL

fabricante / nombre comercial

Cerilliant®

técnicas

gas chromatography (GC): suitable

aplicaciones

forensics and toxicology

Formato

neat

temp. de almacenamiento

−20°C

cadena SMILES

CN(C(=O)C(F)(F)F)[Si](C)(C)C(C)(C)C

InChI

1S/C9H18F3NOSi/c1-8(2,3)15(5,6)13(4)7(14)9(10,11)12/h1-6H3

Clave InChI

QRKUHYFDBWGLHJ-UHFFFAOYSA-N

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Aplicación


  • Pharmaceutical substances in ambient particulates: A preliminary assessment.: This study explores the presence of pharmaceutical compounds in environmental particulate matter, using analytical methods that could involve derivatization agents like MTBSTFA. The detection of these substances in air samples suggests potential health impacts and environmental persistence (Cecinato et al., 2017) (Cecinato et al., 2017).


Información legal

CERILLIANT is a registered trademark of Merck KGaA, Darmstadt, Germany

Pictogramas

FlameExclamation mark
GHS02,GHS07

Palabra de señalización

Warning

Frases de peligro

H226,H315,H319

Clasificaciones de peligro

Eye Irrit. 2 - Flam. Liq. 3 - Skin Irrit. 2

Código de clase de almacenamiento

3 - Flammable liquids

Clase de riesgo para el agua (WGK)

WGK 3

Punto de inflamabilidad (°F)

113.0 °F - closed cup

Punto de inflamabilidad (°C)

45 °C - closed cup

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Certificados de análisis (COA)

Lot/Batch Number

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Sigma-Aldrich

226904

Methoxyamine hydrochloride

(±)-MDA-D5 solution 100 μg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

Supelco

M-010

(±)-MDA-D5 solution

Xiaodong Huang et al.
Analytical chemistry, 80(1), 107-114 (2007-12-07)
This work describes an approach to differential metabolomics that involves stable isotope labeling for relative quantification as part of sample analysis by two-dimensional gas chromatography/mass spectrometry (GCxGC/MS). The polar metabolome in control and experimental samples was extracted and differentially derivatized
Claude Schummer et al.
Talanta, 77(4), 1473-1482 (2008-12-17)
In this study, MTBSTFA and BSTFA, which are among the preferred derivatization reagents for silylation were both tested on derivatization of six different groups of polar chemicals to get information about usefulness in terms of sensitivity and specificity of both
A Royer et al.
Journal of chromatography. A, 1108(1), 129-135 (2006-01-31)
An analytical method has been developed for the determination of residues of ethephon (2-chloroethyl phosphonic acid) in drinking and surface water. The procedure is based on de-ionisation with an anion/cation-exchange resin, solid phase extraction by means of anion-exchange polystyrene-divinylbenzene extraction
Xiaowei Wang et al.
Analytica chimica acta, 753, 57-63 (2012-10-31)
A sample preparation method for the determination of hydroxylated polycyclic aromatic hydrocarbons (OH-PAHs) in sediment samples was developed using gas chromatography-mass spectrometry (GC-MS). Dispersive liquid-liquid microextraction (DLLME) with derivatization was performed following the subcritical water extraction (SWE) that provided which
Man-Jeong Paik et al.
Journal of chromatography. B, Analytical technologies in the biomedical and life sciences, 821(1), 94-104 (2005-05-17)
Simultaneous profiling analysis of urinary amino acids (AAs) and carboxylic acids (CAs) was combined with retention index (I) analysis for graphic recognition of abnormal metabolic state. The temperature-programmed I values of the AA and CA standards measured as ethoxycarbonyl (EOC)/methoxime
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