KITALYSIS-RCM

KitAlysis^™ High-Throughput Medium (5, 6, 7) Ring Closing Metathesis Reaction Screening Kit - Pack of 2

• UNSPSC-Code: 12161600
• NACRES: NA.22

Eigenschaften

• Eignung der Reaktion: core: palladium; reaction type: Buchwald-Hartwig Cross Coupling Reaction; reaction type: Heck Reaction; reaction type: Hiyama Coupling; reaction type: Negishi Coupling; reaction type: Sonogashira Coupling; reaction type: Stille Coupling; reaction type: Suzuki-Miyaura Coupling
• Lagertemp.: 2-8°C

Beschreibung

Anwendung

Screening kit for ring closing metathesis. Step-by-step user guides and a downloadable experimental excel sheets are provided in the below hyperlinks.

Step-by-Step Guide for Ring Closing Metathesis/Cross Metathesis Reaction Screening Kit

Downloadable experimental excel file

Each kit contains 2 customizable screening sets that include the following components:

• 6x4 pre-weighed catalysts in glass microvials loaded with stir bars and topped with cap mat.
• 2 (2 mL) ampules each of of ClPh, PhMe, i-PrOAc, Me-THF, and TFA.
• 1 KitAlysis 24-well reaction block replacement film.
• 4 empty substrate stock solution reaction vials with stir bars.
• 1 internal standard.

Monitor reaction progress via TLC-MS by following this protocol

Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).

Leistungsmerkmale und Vorteile

• Designed and tested by synthetic chemists.
• Easily run 24-microscale reaction in parallel.
• 20 μmol reactions with 1 μmol catalyst (5 mol%), 0.2 M concentration, and optional TFA additive.
• Customizable and downloadable excel template for quick calculations and easy incorporation into electronic laboratory notebooks.

Rechtliche Hinweise

KitAlysis is a trademark of Sigma-Aldrich Co. LLC

Nur Kit-Komponenten

• SnapIT Ampule Opener, Regular, for 1-2ml, 5-10ml, 10-15ml ampoules 1 EA

Kit-Komponenten auch einzeln erhältlich

• 569747 Grubbs Catalyst^® M204, Umicore 3 µmol
• 569755 Hoveyda-Grubbs Catalyst^® M720, Umicore, 97% 3 µmol
• 579726 Grubbs Catalyst^® M102, Umicore, 97% 3 µmol
• 682365 Grubbs Catalyst^® M207, Umicore 3 µmol
• 682373 Hoveyda-Grubbs Catalyst^® M721, Umicore 3 µmol
• 729345 Hoveyda-Grubbs Catalyst^® M722, Umicore 3 µmol
• 900519 Isopropyl acetate, anhydrous, ZerO₂^®, ≥99.6% 8 mL
900520 2-Methyltetrahydrofuran, anhydrous, contains 250 ppm BHT as stabilizer, ZerO₂^®, ≥99.0% 8 mL
900521 Chlorobenzene, anhydrous, ZerO₂^®, 99.8% 8 mL
900522 Toluene, anhydrous, ZerO₂^®, 99.8% 8 mL
Z118850 Spinbar^® magnetic stirring fleas, red, L 10 mm, diam. 3 mm 1 EA

Alle anzeigen (11)

Sicherheitshinweise

• Piktogramme: GHS02,GHS08,GHS05,GHS07,GHS09
• Signalwort: Danger
• H-Sätze: H225,H302 + H332,H304,H315,H318,H335,H336,H361d,H373,H410
• P-Sätze: P210 - P273 - P280 - P301 + P310 - P305 + P351 + P338 - P331
• Gefahreneinstufungen: Acute Tox. 4 Inhalation - Acute Tox. 4 Oral - Aquatic Acute 1 - Aquatic Chronic 1 - Asp. Tox. 1 - Eye Dam. 1 - Flam. Liq. 2 - Repr. 2 - Skin Irrit. 2 - STOT RE 2 Inhalation - STOT SE 3
• Zielorgane: Central nervous system, Respiratory system
• Zusätzliche Gefahrenhinweise: EUH019
• Lagerklassenschlüssel: 3 - Flammable liquids
• WGK: WGK 3