LC/MS Analysis of Ancymidol Enantiomers on Astec® CYCLOBOND I 2000 HP-RSP
CONDITIONS
column
CYCLOBOND I 2000 HP-RSP, 25 cm x 4.6 mm I.D., 5 μm particles (24024AST)
mobile phase
[A] 5 mM ammonium acetate, pH 6.0; [B] acetonitrile; (80:20, A:B)
flow rate
1 mL/min
column temp.
35 °C
detector
MS (m/z = 257)
injection
5 μL
sample
1 mg/mL in methanol
Descrizione
Note legali
Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
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