GC Analysis of LSD (TMS Derivatives) on SLB^®-5ms

column

SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)

oven

150 C (1.50 min), 20 C/min to 300 C (20 min)

inj. temp.

250 °C

MSD interface

330 °C

scan range

m/z 45-525

carrier gas

helium, 0.7 mL/min constant

injection

0.5 μL pulsed splitless, 30 psi. (0.20 min), purge on (1.5 min), purge flow (50.0 mL/min)

liner

2mm I.D., straight

sample

Derivatized LSD using BSTFA