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Merck

467979

Sigma-Aldrich

1,3-Dithiolan

97%

Synonym(e):

1,3-Dithiacyclopentane

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About This Item

Empirische Formel (Hill-System):
C3H6S2
CAS-Nummer:
Molekulargewicht:
106.21
MDL-Nummer:
UNSPSC-Code:
12352100
PubChem Substanz-ID:
NACRES:
NA.22

Qualitätsniveau

Assay

97%

Brechungsindex

n20/D 1.599 (lit.)

bp

183 °C (lit.)

Dichte

1.235 g/mL at 25 °C (lit.)

Funktionelle Gruppe

thioether

SMILES String

C1CSCS1

InChI

1S/C3H6S2/c1-2-5-3-4-1/h1-3H2

InChIKey

IMLSAISZLJGWPP-UHFFFAOYSA-N

Allgemeine Beschreibung

1,3-Dithiolane ,a sulfur containing heterocyclic building block, is a cyclic thioether. Fragmentation modes of 1,3-oxathiolane under electron-impact have been investigated.

Lagerklassenschlüssel

10 - Combustible liquids

WGK

WGK 3

Flammpunkt (°F)

154.4 °F - closed cup

Flammpunkt (°C)

68 °C - closed cup


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Sylvie Goncalves et al.
Chemical communications (Cambridge, England), 46(31), 5778-5780 (2010-07-06)
A concise and diastereoselective formal total synthesis of triptolide, a natural product with a wide range of biological properties, is described. The key reaction is an unprecedented 6-endo-Trig cationic cyclization of a 2-alkenyl-1,3-dithiolane precursor induced by TMSOTf as Lewis acid.
Alexandra Papanikos et al.
Journal of combinatorial chemistry, 6(2), 181-195 (2004-03-09)
A synthetic strategy for the formation of resin-bound internal alpha-keto amide peptides suitable for protease inhibitor screening on solid support is presented. This general approach is based on the incorporation of alpha-keto amide building blocks during solid-phase peptide synthesis (SPPS).
I M Hussaini et al.
Acta pharmacologica Sinica, 21(10), 897-904 (2001-08-15)
To investigate the effect of a group of novel synthetic dithiolane analogs of lignans and a well characterized platelet-activating factor (PAF) receptor antagonist, L659,989 on PAF-receptor binding, IFN-gamma- and lipopolysaccharide (LPS)-induced NO production, and steady-state inducible nitric-oxide synthase (iNOS) mRNA
Kalevi Pihlaja et al.
Magnetic resonance in chemistry : MRC, 49(7), 443-449 (2011-05-07)
1-Oxo-1,3-dithiolane (4) and its cis- and trans-2-methyl (5,6), -4-methyl (7,8) and -5-methyl (9,10) derivatives were prepared by oxidizing the corresponding 1,3-dithiolanes (1-3) with NaIO(4) in water. The oxides were purified and their isomers separated using thin layer chromatography. The structural
Ionization and dissociation of cyclic ethers and thioethers by electron-impact. A comparison between 1, 3-dioxolane, 1, 3-dithiolane and 1, 3-oxathiolane.
Conde-Caprace G and Collin JE.
Org. Mass Spectrom., 6(4), 415-423 (1972)

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