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Merck
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重要文件

21099-U

Supelco

SE-30(聚甲基硅氧烷)

phase SE-30, bottle of 10 g

同義詞:

GC 固定相

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About This Item

分類程式碼代碼:
23151817
NACRES:
SB.54

agency

meets requirements for USP G2

包裝

bottle of 10 g

參數

temp. range at 50-300 °C

技術

gas chromatography (GC): suitable

基質活性組

SE-30 phase

溶解度

chloroform: soluble

柱類型

packed GC

一般說明

GC methods are divided into two classes depending on the nature of stationary phases; gas-solid chromatography (GSC) and gas-liquid chromatography (GLC). GSC has solid adsorptive material and solute particles are removed from mobile phase by electrostatic forces. GLC has a thin layer of liquid coated or bonded on the surface of an inert particle or on the walls of the column where solute particles are retained in the liquid phase based on their partition coefficients. The primary necessity of a stationary phase is to provide sample separation sustaining phase integrity over a reasonable period of time. It should be stable for the chemical and thermal changes. Selectivity, peak symmetry, analysis time, degree of separation, peak tailing are a few parameters that should be considered before choosing a stationary phase. SE-30 is a dimethyl silicone elastomer. It is widely suitable as liquid phase got GLC.
合成的产品更纯净,分子量范围窄,不含用作 GC 固定相的痕量催化剂或杂质。

應用

SE-30 was used as stationary phase for the analysis of the thiohydantoins using GC. It may also be used as liquid phase in identification of the single polychlorinated biphenyls (PCB) components by comparing their retention indices, using high-resolution thin-film glass capillary gas chromatography coupled with electron-capture detector.

儲存類別代碼

10 - Combustible liquids

水污染物質分類(WGK)

WGK 3

閃點(°F)

Not applicable

閃點(°C)

Not applicable

個人防護裝備

Eyeshields, Gloves


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Analysis of polychlorinated biphenyls (PCB) by glass capillary gas chromatography.
Ballschmiter
Fresenius' Zeitschrift fur Analytische Chemie, 302, 20-31 (1980)
A C Moffat
Journal of chromatography, 113(1), 69-95 (1975-03-12)
The dimethyl silicone elastomer SE-30 has been chosen as the preferred liquid phase for the gas-liquid chromatographic analysis of drugs, and retention index data have been compiled for 480 drugs and commonly occurring chemicals such as plasticisers. The inter-laboratory variation
Analysis of amino acid phenylthiohydantoins by gas chromatography.
J J Pisano et al.
The Journal of biological chemistry, 244(20), 5597-5607 (1969-10-25)
James P. Lodge, Jr.
Methods of Air Sampling and Analysis, 98-98 (1988)
David B. Troy, Paul Beringer
Remington: The Science and Practice of Pharmacy, 605-605 (2006)

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