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重要文件

21104

Supelco

OV-1 硅树脂

phase OV-1, bottle of 10 g

同義詞:

GC 固定相

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About This Item

分類程式碼代碼:
23151817

agency

meets requirements for USP G2

品質等級

包裝

bottle of 10 g

參數

100-350 °C temp. range

技術

gas chromatography (GC): suitable

基質活性組

OV-1 phase

溶解度

chloroform, toluene: soluble

柱類型

packed GC

一般說明

合成的产品更纯净,分子量范围窄,不含用作 GC 固定相的痕量催化剂或杂质。
GC methods are divided into two classes depending on the nature of stationary phases; gas-solid chromatography (GSC) and gas-liquid chromatography (GLC). GSC has solid adsorptive material and solute particles are removed from mobile phase by electrostatic forces. GLC has a thin layer of liquid coated or bonded on the surface of an inert particle or on the walls of the column where solute particles are retained in the liquid phase based on their partition coefficients. The primary necessity of a stationary phase is to provide sample separation sustaining phase integrity over a reasonable period of time. It should be stable for the chemical and thermal changes. Selectivity, peak symmetry, analysis time, degree of separation, peak tailing are a few parameters that should be considered before choosing a stationary phase. OV-1 is suitable for the separation of drugs, alkaloids, phenols and steroids.

應用

OV-1 is suitable as stationary phase for monitoring the urinary excretion in man for pentachlorophenol (PCP) and PCP conjugated to glucuronic acid using gas chromatography with electron capture detection (GC/ECD).

儲存類別代碼

10 - Combustible liquids

水污染物質分類(WGK)

WGK 1

閃點(°F)

214.0 °F - closed cup

閃點(°C)

101.1 °C - closed cup

個人防護裝備

Eyeshields, Gloves


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分析證明 (COA)

Lot/Batch Number

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S Uhl et al.
Archives of toxicology, 58(3), 182-186 (1986-02-01)
Pentachlorophenol (PCP) was given orally to three volunteers at single doses of 3.9, 4.5, 9, and 18.8 mg. Daily urinary excretion of PCP and PCP conjugated to glucuronic acid was monitored using gas chromatography with electron capture detection (GC/ECD). Based
James P. Lodge, Jr.
Methods of Air Sampling and Analysis, 98-98 (1988)
David B. Troy, Paul Beringer
Remington: The Science and Practice of Pharmacy, 605-605 (2006)

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