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KITALYSIS-SM

Sigma-Aldrich

KitAlysis™ 高通量 Suzuki-Miyaura 交叉偶联反应筛选试剂盒 - 4 件装

别名:

Suzuki-Miyaura 交叉偶联

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About This Item

分類程式碼代碼:
12161600
NACRES:
NA.22

反應適用性

reaction type: Cross Couplings
reaction type: Suzuki-Miyaura Coupling
reagent type: catalyst
core: palladium

官能基

phosphine

相关类别

應用

Suzuki-Miyaura 交叉偶联反应筛选试剂盒。下面的超链接提供了逐步用户指南和可下载的实验 excel 表格。
Suzuki-Miyaura 交联反应筛选试剂盒的逐步指南
可下载的实验 excel 表格

每个试剂盒包含 4 个可定制筛选集，包括以下组件：
  • 6 x 4 预称重催化剂，装在带搅拌棒和盖垫的玻璃瓶内
  • 1 (2 mL) 安培瓶，各含甲苯、THF、正丁醇, DMAc 和 aq.1.5 M K3PO4。
  • 4 个新的 KitAlysis 24 孔反应块置换膜。
  • 4 个带搅拌棒的底物反应瓶。
  • 1 个内部标准品。
通过 TLC-MS，按 本方案监控反应进程

最好配合 KitAlysis 使用台式分析箱 and 24 孔反应块（单独销售）。

特點和優勢

  • 由合成化学家设计和测试。
  • 轻松平行运行 24 个微量反应。
  • 含 1 μmol 催化剂、3 等当量碱、0.1 M 浓度进行 10 μmol 反应。
  • 可定制的 Excel 模板，可快速计算，并易于整合到电子实验室笔记本中。

法律資訊

KitAlysis is a trademark of Sigma-Aldrich Co. LLC

仅试剂盒组分

产品编号
说明
  • SnapIT Ampule Opener, Regular, for 1-2ml, 5-10ml, 10-15ml ampoules 1 EA

试剂盒组分也可单独购买

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  • Degassed Potassium phosphate tribasic solution 8 mL
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訊號詞

Danger

危險分類

Acute Tox. 4 Dermal - Acute Tox. 4 Inhalation - Acute Tox. 4 Oral - Aquatic Acute 1 - Aquatic Chronic 1 - Asp. Tox. 1 - Carc. 2 - Eye Dam. 1 - Flam. Liq. 2 - Repr. 1B - Skin Irrit. 2 - STOT RE 2 - STOT SE 3

標靶器官

Central nervous system, Respiratory system

安全危害

EUH019

儲存類別代碼

3 - Flammable liquids

閃點（°F）

1.4 °F

閃點（°C）

-17 °C

分析证书(COA)

输入产品批号来搜索 分析证书(COA) 。批号可以在产品标签上"批“ （Lot或Batch）字后找到。

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High-Throughput Experimentation in Catalysis and Materials Science.
Gordillo A, et al.
Ullmann's Encyclopedia of Industrial Chemistry (2014)
Scientist-Led High-Throughput Experimentation (HTE) and Its Utility in Academia and Industry.
Schmink JR, et al.
Aldrichimica Acta, 46, 71-80 (2013)
Spencer D Dreher et al.
Journal of the American Chemical Society, 130(29), 9257-9259 (2008-06-28)
Microscale parallel experimentation was used to discover three catalyst systems capable of coupling secondary organotrifluoroborates with sterically and electronically demanding aryl chlorides and bromides. The ensuing results represent the first comprehensive study of alkylboron coupling to aryl chlorides and, in
Karl D Collins et al.
Nature chemistry, 6(10), 859-871 (2014-09-23)
New organic reactivity has often been discovered by happenstance. Several recent research efforts have attempted to leverage this to discover new reactions. In this Review, we attempt to unify reported approaches to reaction discovery on the basis of the practical

商品

Scale-Up Guide: Suzuki-Miyaura Cross-Coupling Reaction

All of the preformed catalysts used in the kit are air and moisture stable complexes in their commercially available form.

Scale-Up Guide: Suzuki-Miyaura Cross-Coupling Reaction

All of the preformed catalysts used in the kit are air and moisture stable complexes in their commercially available form.

KitAlysis™ High-Throughput Screening Platform

KitAlysis High-Throughput Screening Kits provide solution to efficiently identify or optimize suitable catalytic reaction conditions. Chemist can rapidly run 24 unique micro scale reactions in parallel with tailored conditions.

KitAlysis™ High-Throughput Screening Platform

KitAlysis High-Throughput Screening Kits provide solution to efficiently identify or optimize suitable catalytic reaction conditions. Chemist can rapidly run 24 unique micro scale reactions in parallel with tailored conditions.

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实验方案

Step-by-Step Guide for KitAlysis™ Suzuki-Miyaura Cross-Coupling Reaction Screening Kit

A step-by-step protocol guide for KitAlysis Suzuki-Miyaura Cross-Coupling Reaction Screening Kit.

相关内容

Reaction Design & Optimization
Reaction Design & Optimization

Chemical reaction design and optimization in organic synthesis aims to precisely alter reaction parameters to achieve optimum results in finding pathways to target molecules.

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