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Key Documents

G003580

US EPA Method 8082: GC Analysis of Aroclor 1016/1260 (PCBs) on SLB®-5ms

suitable for GC

Synonym(s):

28471-U, 46846-U, Aroclor, US EPA Method 608

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About This Item

technique(s)

gas chromatography (GC): suitable

test parameters

column: SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)
oven: 100 °C (2 min), 15 °C/min to 330 °C (3 min)
inj. temp.: 250 °C
detector: ECD, 330 °C
carrier gas: helium, 25 cm/sec, constant
injection: 2 μL splitless (0.75 min)
liner: 4 mm I.D., single taper
sample: Aroclor standard mix 1 (46846-U) diluted to 500 ppb / 50 ppb (Aroclors / surrogates) in n-hexane

application(s)

environmental

Analysis Note

Aroclors are commercial mixtures of PCB congeners. Due to their stability, they ave been used in many different industrial and commercial applications. Because of their toxicity and ability to bioaccumulate, production of these materials ceased in 1977. This application demonstrates the separation of two common Aroclor mixtures, Aroclor 1016 and Aroclor 1260 on the SLB-5ms.

Legal Information

SLB is a registered trademark of Merck KGaA, Darmstadt, Germany

Analyte

Description

    Aroclor 1016
    Aroclor 1260

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