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Merck
  • Hydroxyapatite coatings on nanotubular titanium dioxide thin films prepared by radio frequency magnetron sputtering.

Hydroxyapatite coatings on nanotubular titanium dioxide thin films prepared by radio frequency magnetron sputtering.

Journal of nanoscience and nanotechnology (2013-07-26)
Jinho Shin, Kwangmin Lee, Jeongtae Koh, Hyeju Son, Hyunseung Kim, Hyun-Pil Lim, Kwidug Yun, Gyejeong Oh, Seokwoo Lee, Heekyun Oh, Kyungku Lee, Gabwoon Hwang, Sang-Won Park
要旨

In this study, hydroxyapatite (HA) was coated on anodized titanium (Ti) surfaces through radio frequency magnetron sputtering in order to improve biological response of the titanium surface. All the samples were blasted with resorbable blasting media (RBM). RBM-blasted Ti surface, anodized Ti surface, as-sputtered HA coating on the anodized Ti surface, and heat-treated HA coating on the anodized Ti surface were prepared. The samples were characterized using scanning electron microscopy and X-ray photoemission spectroscopy, and biologic responses were evaluated. The top of the TiO2 nanotubes was not closed by HA particles when the coating time is less than 15 minutes. It was demonstrated that the heat-treated HA was well-crystallized and this enhanced the cell attachment of the anodized Ti surface.

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Sigma-Aldrich
チタン, powder, <45 μm avg. part. size, 99.98% trace metals basis
Sigma-Aldrich
チタン, foil, thickness 0.127 mm, 99.7% trace metals basis
Sigma-Aldrich
チタン, foil, thickness 0.25 mm, 99.7% trace metals basis
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チタン, powder, −100 mesh, 99.7% trace metals basis
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チタン, wire, diam. 0.25 mm, 99.7% trace metals basis
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チタン, sponge, 3-19 mm, 99.5% trace metals basis
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チタン, foil, thickness 2.0 mm, 99.7% trace metals basis
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チタン, foil, thickness 0.025 mm, 99.98% trace metals basis
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ヒドロキシアパタイト, puriss., meets analytical specification of Ph. Eur., BP, FCC, E341, ≥90% (calculated on glowed substance)
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チタン, foil, thickness 0.5 mm, 99.99% trace metals basis
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チタン, sputtering target, diam. × thickness 2.00 in. × 0.25 in., 99.995% trace metals basis
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チタン, wire, diam. 1.0 mm, 99.99% trace metals basis
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チタン, 5-10 mm, ≥99.99% trace metals basis (purity exclusive of Na and K content)
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ヒドロキシアパタイト, purum p.a., ≥90% (as Ca3(PO4)2, KT)
Sigma-Aldrich
チタン, foil, thickness 0.127 mm, ≥99.99% trace metals basis
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チタン, foil, thickness 0.25 mm, 99.99% trace metals basis
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ヒドロキシアパタイト, SAJ first grade, 98.0-103.0%
Sigma-Aldrich
チタン, wire, diam. 0.81 mm, 99.7% trace metals basis
Sigma-Aldrich
チタン, wire, diam. 0.5 mm, 99.99% trace metals basis
Sigma-Aldrich
ヒドロキシアパタイト, Type I, buffered aqueous suspension
Sigma-Aldrich
チタン, evaporation slug, diam. × L 6.3 mm × 6.3 mm, ≥99.99% trace metals basis
チタン, IRMM®, certified reference material, 0.1 mm foil
チタン, IRMM®, certified reference material, 0.5 mm foil
チタン, IRMM®, certified reference material, 0.5 mm wire