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Safety Information

52779-U

Supelco

Supelclean Ultra 2400 solid phase extraction (SPE) Tubes

volume 1 mL, pkg of 108

Synonym(s):

Supelclean™ Ultra

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About This Item

UNSPSC Code:
41115712
NACRES:
NB.21

product name

Supelclean Ultra 2400, volume 1 mL, pkg of 108

product line

Supelclean™

Quality Level

100

composition

bed A, 120 mg
bed B, 100 mg (Z-Sep)

packaging

pkg of 108

technique(s)

solid phase extraction (SPE): suitable

volume

1 mL

matrix active group

C18 coating
Carbon coating
PSA coating

application(s)

food and beverages

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General description

Supelclean™ PSA, Discovery® C18, and Spherical Carbon
This multi-bed solid phase extraction (SPE) cartridge was designed for the cleanup of extracts of difficult matrices such as dry commodities (tea, spices, coffee, etc.) prior to pesticide residue analysis, typically performed by GC/MSMS and LC/MS/MS. These types of samples can contain pigments and oils, and may not be sufficiently cleaned using a standard QuEChERS cleanup.
The top bed consists of a mixture of PSA/C18 and a graphitized, spherical carbon. PSA removes acidic interferences, C18 retains some hydrophobic interferences, and carbon removes pigments. The variety of carbon used in this cartridge was engineered to remove sufficient pigmentation while allowing for better recoveries of compounds with planar structures. The bottom bed of the cartridge contains Z-Sep, which is a zirconia-coated silica. Z-Sep removes oily residues, and provides additional pigment removal.
The cartridge can be used for cleanup of acetonitrile extracts to be analyzed by either GC or HPLC.

Legal Information

Discovery is a registered trademark of Merck KGaA, Darmstadt, Germany
Supelclean is a trademark of Sigma-Aldrich Co. LLC

Pictograms

CorrosionExclamation mark
GHS05,GHS07

Signal Word

Danger

Hazard Statements

H317,H318

Hazard Classifications

Eye Dam. 1 - Skin Sens. 1

Storage Class Code

11 - Combustible Solids

WGK

WGK 3

Flash Point(F)

Not applicable

Flash Point(C)

Not applicable

Regulatory Listings

Regulatory Listings are mainly provided for chemical products. Only limited information can be provided here for non-chemical products. No entry means none of the components are listed. It is the user’s obligation to ensure the safe and legal use of the product.

JAN Code

52779-U:

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Certificates of Analysis (COA)

Lot/Batch Number
16807603
16807601
15981602
15981601
14697403

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Articles

Improved Recoveries and Lower Background for GC/MS/MS and LC/MS/MS Analysis of Pesticides in Green Tea

A procedure for cleanup of green tea extracts provides low background and allowed for the analysis of more pesticides at lower levels than QuEChERS. Uses less solvents and no toluene.

Analysis of Pesticides in Turmeric Powder by LC/MS/MS and GC/MS/MS after Cleanup with Dual-Layer SPE Cartridge

Pesticide residue testing of turmeric and other (dried) spices is challenging due to their complex compositions and high matrix. An efficient SPE clean-up can be achieved by a new Dual-layer cartridge.

Analysis of Pesticide Residues in Ginger Powder Using QuEChERS Extraction and Clean-up with a Novel Dual Layer SPE Cartridge

The odor and pungency of ginger is due to the presence of terpenes, gingerols and shogaols. These compounds contribute to the highly complex matrix of ginger, which subsequently presents a challenge in low level analyses of contaminants. A novel 2-layer SPE cartridge efficiently reduces background for pesticide determination.

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