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GC Analysis of Amines in Water on SPB®-1 SULFUR after SPME using 65 μm PDMS/DVB Fiber

GC Analysis of Amines in Water on SPB®-1 SULFUR after SPME using 65 μm PDMS/DVB Fiber suitable for GC, application for SPME

Materiali

Colonna analitica

N° Catalogo
Descrizione
Determinazione del prezzo

24158

SPB®-1 SULFUR Capillary GC Column

L × I.D. 30 m × 0.32 mm, df 4.00 μm

Fibra per SPME

N° Catalogo
Descrizione
Determinazione del prezzo

57310-U

Gruppo fibre SPME polidimetilsilossano/divinilbenzene (PDMS/DVB)

df 65 μm(PDMS/DVB, needle size 24 ga, for use with manual holder

CONDITIONS

sample/matrix

amines at 5 ppm in water, 27% NaCl, pH 9.5

SPME fiber

65 μm polydimethylsiloxane/divinylbenzene (57310)

extraction

20 min, fiber immersed in water, rapid stirring

desorption process

270 °C for 5 min

column

SPB®-1 SULFUR, 30 m × 0.32 mm I.D., 4.0 μm (24158)

oven

50 °C (2 min), 10 °C/min to 150 °C

inj. temp.

270 °C

detector

MSD, SIM at 0.6 sec/scan

carrier gas

helium, 25 cm/sec (set @ 50 °C)

liner

0.75 mm I.D., SPME

Descrizione

Note legali

SPB is a registered trademark of Merck KGaA, Darmstadt, Germany

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Related Product Categories

HPLC ColumnsGC Columns & AccessoriesTLC Plates & AdsorbentsSolid Phase Microextraction (SPME)Solid Phase Extraction & QuEChERS

Related Applications

Small Molecule HPLCLarge Molecule HPLCGas Chromatography (GC)TLCSolid Phase Microextraction (SPME)Solid Phase Extraction (SPE)QuEChERS