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Supelco

Colonna GC capillare SPB®-5

L × I.D. 30 m × 0.53 mm, df 5.00 μm

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About This Item

Codice UNSPSC:
41115710
eCl@ss:
32119290

Materiali

fused silica

agenzia

meets requirements for USP G27 and G36

Parametri

-60-260 °C temperature (isothermal)
-60-280 °C temperature (programmed)

Beta

27

df

5.00 μm

tecniche

gas chromatography (GC): suitable

Lungh. × D.I.

30 m × 0.53 mm

Gruppo funzionale matrice

Bonded; poly(5% diphenyl/95% dimethyl siloxane) phase

Tipo di colonna

capillary non-polar

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Descrizione generale

Capillary GC column is also known as open tubular column. The carrier gas flows through the central aperture and is unrestricted throughout the length of the column.
Applicazione: Questa colonna non polare per scopi generali offre principalmente un ordine di eluizione secondo il punto di ebollizione con un piccolo aumento di selettività, specialmente per i composti aromatici.
Codice USP: questa colonna soddisfa i requisiti USP G27 e G36.
Fase
  • Legata
  • Poli (5% difenile/95% dimetilsilossano)
Limiti di temperatura:
  • ≤D. I. 0,32 mm, <2 μm: da -60 °C a 320 °C (isoterma o programmata)
  • ≤D. I. 0,32 mm, ≥2 μm: da -60 °C a 300 °C (isoterma o programmata)
  • ≥D. I. 0,53 mm, <2 μm: da -60 °C a 300 °C (isoterma) o 320 °C (programmata)
  • ≥D. I. 0,53 mm, ≥2 μm: da -60 °C a 260 °C (isoterma) o 280 °C (programmata)

Applicazioni

SPB®-5 Capillary GC Column was used for speciation of the nitrogen compounds (quantitatively), which are polar and somewhat basic in nature, with chemiluminescence detection. It may be used as stationary phase for determination of nivalenol and deoxynivalenol in cereals by electron-capture gas chromatography. It may also find application in being used as stationary phase in capillary column gas chromatography for determination of sterols.

Altre note

We offer a variety of chromatography accessories including analytical syringes

Note legali

SPB is a registered trademark of Merck KGaA, Darmstadt, Germany

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Determination of nivalenol and deoxynivalenol in cereals by electron-capture gas chromatography.
Scott PM
Journal - Association of Official Analytical Chemists, 69 (5), 889-893 (1985)
O Suzuki et al.
Forensic science international, 46(3), 169-180 (1990-07-01)
Positive-ion electron impact (PIEI), positive-ion chemical ionization (PICI) and negative-ion chemical ionization (NICI) mass spectra of 9 carbamate pesticides are presented. In the PIEI mode, the spectra showed small molecular peaks, intense or base peaks due to M - CH3NHCO
Luisito Cercaci et al.
Journal of chromatography. A, 985(1-2), 211-220 (2003-02-13)
The sterol composition of extra virgin olive oil is very characteristic and, thus, has become a helpful tool to detect adulterations with other vegetable oils. Special attention has been addressed to the separate determination of the free and esterified sterol
J M Jurado et al.
Talanta, 106, 14-19 (2013-04-20)
4-Methylsterols and 4,4-dimethylsterols of 47 samples of subcutaneous fat from Iberian pigs reared on two different fattening systems, "Extensive" and "Intensive", have been analyzed by GC-MS and GC-FID. The lipids were extracted by melting the subcutaneous fat in a microwave
Zhihua Fan et al.
Environmental science & technology, 40(19), 6051-6057 (2006-10-21)
A sensitive, simple, and cost-effective passive sampling methodology was developed to quantify personal exposure to gaseous polycyclic aromatic hydrocarbons (PAHs). A Fan-Lioy passive PAH sampler (FL-PPS) is constructed from 320 sections of 1-cm long SPB-5 GC columns (0.75-mm i.d. and

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