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材料
PE frit (20 μm)
polypropylene hardware
品質
MS Friendly
成份
bed wt., 30 mg/well
包裝
pk of 1
技術
solid phase extraction (SPE): suitable
表面積
160-420 m2/g
基質
Sulfonic acid functionalized hydrophilic modified styrene polymer particle platform
基質活性組
sulfonic acid phase
粒徑
50-70 μm
孔徑
80-200 Å pore size
應用
food and beverages
分離技術
ion exchange
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一般說明
Sample Matrix Compatibility: Aqueous solutions (biological fluids, water)
- Sulfonic acid functionalized hydrophilic modified styrene polymer
- Developed for the extraction of a highly broad range of compounds from aqueous samples
- Retention predominately based on ion-exchange; however, because the phase is hydrophilic modified, it is amenable to polar compounds as well.
特點和優勢
- 价格低廉但具有出色的样品制备性能
- 可用于通用方法 — 在方法开发时省时、成本低并减少麻烦
- 容量更大，床重更轻 = 洗脱体积更小 = 处理样品更迅速
- 能忍受过度干涸，可用于更极端条件的方法
- 低紫外和质谱可提取物，背景更低，灵敏度更高
- 严格的生产和质量控制原则提供更好的批次之间、管之间以及孔之间的一致性，能获得更好的准确度和精度
法律資訊
訊號詞
Warning
危險分類
Eye Irrit. 2 - Skin Irrit. 2 - STOT SE 3
標靶器官
Respiratory system
儲存類別代碼
11 - Combustible Solids
水污染物質分類（WGK）
WGK 3
閃點（°C）
Not applicable
商品
Separation of S(+)-Amphetamine (dextro-Amphetamine) solution, 1.0 mg/mL in methanol, ampule of 1 mL, certified reference material; R(-)-Amphetamine (levo-Amphetamine), 1.0 mg/mL in methanol, ampule of 1 mL, certified reference material
Shown here is the chiral separation of amphetamine enantiomers under MS-compatible conditions on Astec CHIROBIOTIC® V2 after extraction from urine using Supel™-Select SCX SPE 96-well plates. The highest grade mobile phase solvents and additives were used to supply low background interference and low particulate contaminants for robust, trouble-free operation. Cerilliant CRMs provided reliable identification and quantification.
SPE retention mechanism in this case is based on the electrostatic attraction of charged functional groups of the analyte(s) to oppositely charged functional groups on the sorbent.
SPE retention mechanism in this case is based on the electrostatic attraction of charged functional groups of the analyte(s) to oppositely charged functional groups on the sorbent.
实验方案
In this study, optimized methods are presented for sample preparation and chiral chromatography for the LC/MS analysis of amphetamine and methamphetamine enantiomers in urine.
Optimized sample prep and chiral chromatography methods for the LC/MS analysis of these drug enantiomers in urine
LC/MS Analysis of Methamphetamine Enantiomers on Astec® CHIROBIOTIC® V2 in Urine after SPE using Supel™-Select SCX
Retention occurs through polar interaction between the sorbent and analytes. Typical sample matrices that can be employed in normal-phase SPE include hydrocarbon or fatty oils diluted in a solvent like hexane, isooctane, chlorinated solvent, THF, diethyl ether, or ethyl acetate.
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