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Key Documents

57221-U

Supelco

Discovery® DSC-SCX 固相萃取散装填料

pkg of 100 g

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About This Item

分類程式碼代碼:
41115712
NACRES:
NB.21

包裝

pkg of 100 g

技術

solid phase extraction (SPE): suitable

基質活性組

sulfonic acid bonding

應用

food and beverages

分離技術

ion exchange

一般說明

助留机理:阳离子交换
样品基质相容性:有机溶液或水溶液

  • 多点键合的苯磺酸官能团,pKa (< 1.0)
  • 反离子为 H+
  • 硅胶基体可与强有机溶剂一起使用(不会收缩/溶胀)
  • 极好的离子交换容量用于净化组合化学反应的溶液相(0.8 毫当量/克)(从反应副产物和多余试剂中移除目标分子)
  • 苯环的存在提供了从水性基质中萃取阳离子时应考虑的某些混合模式能力(疏水相互作用)

法律資訊

Discovery is a registered trademark of Merck KGaA, Darmstadt, Germany

象形圖

CorrosionExclamation mark

訊號詞

Danger

危險聲明

危險分類

Aquatic Chronic 3 - Eye Dam. 1 - Skin Corr. 1A - Skin Sens. 1

儲存類別代碼

8A - Combustible corrosive hazardous materials

水污染物質分類(WGK)

WGK 3

閃點(°F)

Not applicable

閃點(°C)

Not applicable


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SPE retention mechanism in this case is based on the electrostatic attraction of charged functional groups of the analyte(s) to oppositely charged functional groups on the sorbent.

SPE retention mechanism in this case is based on the electrostatic attraction of charged functional groups of the analyte(s) to oppositely charged functional groups on the sorbent.

实验方案

Melamine was extracted from milk using Supelco® Discovery® DSC-SCX SPE tubes. Analysis was performed by HPLC, using an Ascentis® Express HILIC column.

Retention occurs through polar interaction between the sorbent and analytes. Typical sample matrices that can be employed in normal-phase SPE include hydrocarbon or fatty oils diluted in a solvent like hexane, isooctane, chlorinated solvent, THF, diethyl ether, or ethyl acetate.

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