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T-019

Supelco

(−)-11-nor-9-羧基-Δ9-THC 溶液

1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

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About This Item

经验公式（希尔记法）:
C21H28O4
CAS号:
56354-06-4
分子量:
344.44
EC號碼:
200-659-6
MDL號碼:
MFCD02682121
分類程式碼代碼:
41116107
PubChem物質ID:
329826590
NACRES:
NA.24

等級

certified reference material

品質等級

300

形狀

liquid

特點

Snap-N-Spike®/Snap-N-Shoot®

包裝

ampule of 1 mL

製造商／商標名

Cerilliant®

drug control

psicótropo (Spain); Decreto Lei 15/93: Tabela IIB (Portugal)

濃度

1.0 mg/mL in methanol

技術

gas chromatography (GC): suitable
liquid chromatography (LC): suitable

適合性

suitable for immunoassay

應用

cannabis testing
forensics and toxicology

格式

single component solution

儲存溫度

−20°C

SMILES 字串

CCCCCC(C=C1O)=CC2=C1[C@@]3([H])[C@@](C(C)(C)O2)([H])CCC(C(O)=O)=C3

InChI

1S/C21H28O4/c1-4-5-6-7-13-10-17(22)19-15-12-14(20(23)24)8-9-16(15)21(2,3)25-18(19)11-13/h10-12,15-16,22H,4-9H2,1-3H3,(H,23,24)/t15-,16-/m1/s1

InChI 密鑰

YOVRGSHRZRJTLZ-HZPDHXFCSA-N

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相关类别

一般說明

11-nor-9-羧基-Δ9-THC 是 11-羟基-Δ9-四氢大麻酚的非活性羧基形式，后者是大麻 Δ9-四氢大麻酚（Δ9-THC）主要精神活性成分的主要氧化代谢物。

應用

该认证加标溶液® 适用于通过 HPLC、GC/MS 或 LC-MS/MS 法进行 (−)-11-nor-9-羧基-Δ9-THC 测试，从而用于法医分析、临床毒理学、尿液药物测试和大麻效力或杂质分析测试等应用。该认证标准物质（CRM）还可作如下用途：
  • 通过气相色谱（GC）联合三重四极杆质谱仪分析血浆和尿液中 Δ9-四氢大麻酚（Δ9-THC）及其三种代谢物
  • 开发基于固相萃取（SPE）的自动样品制备方法，以使用液相色谱-质谱法（LC-MS）测定血清、唾液和尿液中 ∆9-四氢大麻酚（THC）及其三种主要代谢物
  • 通过大气压化学电离气相色谱-串联质谱法（APGC-MS/MS）同时测定人血清样品中的大麻素及其代谢物
  • 通过气相色谱（GC）联合真空 UV 光谱法进行大麻素及其代谢产物的多重分析
  • 基于液相色谱-串联质谱（LC-MS/MS）法在固相萃取（SPE）后测定口服液样品中的 10 种大麻素
  • 通过固相萃取（SPE）和 LC-MS/MS 对 14 种不同类别滥用药物进行多残留分析

特點和優勢

  • 完全符合 ISO/IEC 17025 和 ISO 17034 认证
  • 附综合分析证书（CoA），包括稳定性、均匀性、浓度准确性、不确定性和可追溯性数据
  • 通过实时稳定性研究严格测试，以确保准确性和保质期
  • 使用合格的精密天平进行重量准备，以确保最小不确定性
  • 氩气环境下火焰密封，装入安瓿以便长期保存
  • 提供方便的 DEA 豁免格式，以提高实验室效率

法律資訊

CERILLIANT is a registered trademark of Merck KGaA, Darmstadt, Germany
CERTIFIED SPIKING SOLUTION is a registered trademark of Cerilliant Corporation
Snap-N-Shoot is a registered trademark of Cerilliant Corporation
Snap-N-Spike is a registered trademark of Merck KGaA, Darmstadt, Germany

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T-004

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T-005

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T-006

(±)-Δ-四氢大麻酸标准液 溶液, 100 μg/mL in methanol, ampule of 1 mL, Cerilliant®

T-007

(±)-11-nor-9-Carboxy-Δ9-THC-D9 solution, 100 μg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

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T-011

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T-018

(−)-11-nor-9-羧基-Δ9-THC 溶液, 100 μg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

T-038

(+)-11-去甲-Δ9-THC-9-羧酸葡糖苷酸 溶液, 100 μg/mL in methanol, ampule of 1 mL, Cerilliant®

T-080

(±)-cis-11-Nor-9-carboxy-Δ9-THC-D3 glucuronide solution, 100 μg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

T-148

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訊號詞

Danger

危險分類

Acute Tox. 3 Dermal - Acute Tox. 3 Inhalation - Acute Tox. 3 Oral - Flam. Liq. 2 - STOT SE 1

標靶器官

Eyes

儲存類別代碼

3 - Flammable liquids

水污染物質分類（WGK）

WGK 1

閃點（°F）

49.5 °F - closed cup

閃點（°C）

9.7 °C - closed cup

分析证书(COA)

输入产品批号来搜索 分析证书(COA) 。批号可以在产品标签上"批“ （Lot或Batch）字后找到。

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Yannick Lecompte et al.
Journal of analytical toxicology, 36(8), 569-574 (2012-08-31)
The guidelines for screening of urinary cannabinoids require that all specimens testing positive should be confirmed by gas chromatography-mass spectrometry at a confirmatory test cutoff value of 15 ng/mL of 11-nor-9-carboxy-Δ9-tetrahydrocannabinol (THCCOOH). To assess the impact of lowering the confirmatory
Vanessa de M Prata et al.
Analytical and bioanalytical chemistry, 403(2), 625-632 (2012-03-01)
A new procedure is described for the derivatization by silylation of 11-nor-Δ(9)-tetrahydrocannabinol-9-carboxylic acid (THCCOOH) present in urine, followed by analysis using gas chromatography-tandem mass spectrometry. A conventional procedure for derivatization of the analyte was evaluated using two types of experimental
Iria González-Mariño et al.
Analytical chemistry, 84(3), 1708-1717 (2011-12-22)
For the first time, a mixed-mode solid-phase extraction with fractionation of basic analytes from neutral and acidic species during cartridge elution and liquid chromatography-quadrupole-time-of-flight mass spectrometry (LC-QTOF-MS) was combined for the quantitative determination of 24 illicit drugs and metabolites in
Gabriele Zanchetti et al.
Journal of mass spectrometry : JMS, 47(1), 124-130 (2012-01-28)
A method for the rapid and robust confirmation of 11-nor-∆9-tetrahydrocannabinol-9-carboxylic acid (THCA) in urine involving basic hydrolysis with NaOH and direct injection of the hydrolysate in a column-switching LC-MS-MS system was developed and validated. THCA-d3 was used as internal standard.
Cynthia Coulter et al.
Journal of analytical toxicology, 36(6), 413-417 (2012-04-26)
This paper describes the determination of tetrahydrocannabinol (THC) and its metabolite, 11-nor-Δ⁹-tetrahydrocannabinol-9-carboxylic acid (THC-COOH) in oral fluid using solid-phase extraction and liquid chromatography with tandem mass spectral detection (LC-MS-MS) and its application to proficiency specimens. The method employs collection of
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实验方案

LC/MS (TOF) Analysis of Drugs and Their Glucuronide Metabolites in Urine on Titan™ C18 after Solid Phase Extraction (SPE) using Supel™-Select SCX, β-Glucuronidase Enzyme Digestion

-THC solution, 1.0 mg/mL in methanol, ampule of 1 mL, certified reference material

Using UHPLC/MS (TOF) for Detection of Drugs and Metabolites in Urine Following Optimized Enzymatic Hydrolysis Conditions

To optimize hydrolysis using β-glucuronidase, factors such as incubation time, temperature, hydrolysis pH, enzyme source, and enzyme concentration must be evaluated for each glucuronide metabolite to be analyzed.

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