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反應適用性
reaction type: Buchwald-Hartwig Cross Coupling Reaction
reaction type: Heck Reaction
reaction type: Hiyama Coupling
reaction type: Negishi Coupling
reaction type: Sonogashira Coupling
reaction type: Stille Coupling
reaction type: Suzuki-Miyaura Coupling
品質等級
一般說明
提供惰性环境，以在实验室通风橱中进行氧敏感的交叉偶联反应。
设计用于与KitAlysis高通量筛选试剂盒一起使用。
组件：
- Ι惰性盒
- 24孔反应块
- 带有钻头的扭力螺丝刀
- 反应块替换螺丝（10个）
特點和優勢
- 在惰性环境下平行进行24次微量级反应。
- 在工作区域提供恒定的惰性气流。
- 易于从惰性气体阀门或独立气罐上连接管道（不包括在内）
24孔反应块和螺丝刀套组
- 扭力螺丝刀专门设计用于对反应块进行密封，以便在高温下加热时减少溶剂的损失。
- 扭矩设置可防止过度拧紧和剥离螺丝。
- 其中包括小螺丝刀，可在反应完成后轻松取下拧紧的螺丝。
法律資訊
也與該產品經常一起購買
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KitAlysis High-Throughput Screening Kits provide solution to efficiently identify or optimize suitable catalytic reaction conditions. Chemist can rapidly run 24 unique micro scale reactions in parallel with tailored conditions.
KitAlysis High-Throughput Screening Kits provide solution to efficiently identify or optimize suitable catalytic reaction conditions. Chemist can rapidly run 24 unique micro scale reactions in parallel with tailored conditions.
Multiple tools have been created to ensure your success with kit set up. Start with the more detailed guide to ensure you are comfortable with all of the steps before using the quick guides on the excel worksheet. Remember that while the technique is new, it is still organic chemistry and so the steps will seem easy once you try just one kit. It is just a new way of approaching something you are already very good at.
The PhotoKitAlysis Reaction Kit was designed to provide the best possible chance of finding good reaction conditions for cross-coupling reactions: pre-weighed base or base solution (provided), 10–20 mmol coupling partner (user supplied), 10 mmol aryl halide substrate (user supplied), Catalysts (user supplied), 6 solvents (toluene, DMA. THJF, n-butanol, MeOH, MeCN) (provided).
实验方案
Solutions & slurries to make: Go to the online user set-up page to enter molecular weights into the downloadable excel file.
A step-by-step protocol guide for KitAlysis Suzuki-Miyaura Cross-Coupling Reaction Screening Kit.
Catalyst screening, KitAlysis™ High-Throughput Screening Kits, Thin layer chromatography (TLC), parallel analysis, parallel synthesisigh-Throughput Buchwald-Hartwig Amination Reaction Screening Kit, TLC-MS analysis
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